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Sabine Hediger



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Fast magic angle spinning for the characterization of milligram quantities of organic and biological solids at natural isotopic abundance by 13C–13C correlation DNP-enhanced NMR

Adam Smith , Rania Harrabi , Thomas Halbritter , Daniel Lee , Fabien Aussenac
Solid State Nuclear Magnetic Resonance, 2023, 123, pp.101850. ⟨10.1016/j.ssnmr.2022.101850⟩
Journal articles hal-03927273v1
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Optimizing chemistry at the surface of prodrug-loaded cellulose nanofibrils with MAS-DNP

Akshay Kumar , Bastien Watbled , Isabelle Baussanne , Sabine Hediger , Martine Demeunynck
Communications Chemistry, 2023, 6 (1), pp.58. ⟨10.1038/s42004-023-00852-2⟩
Journal articles hal-04049743v1
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Biomolecular and Biological Applications of Solid-State NMR with Dynamic Nuclear Polarization Enhancement

Wing Ying Chow , Gaël de Paëpe , Sabine Hediger
Chemical Reviews, inPress, ⟨10.1021/acs.chemrev.1c01043⟩
Journal articles hal-03658826v1
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Sonocrystallization of CMONS Needles and Nanocubes: Mechanistic Studies and Advanced Crystallinity Characterization by Combining X-ray and Electron Diffractions with DNP-Enhanced NMR

X. Cattoen , Akshay Kumar , Carole Vaillant , Mauricio Matta-Seclén , Fabien Dubois
Crystal Growth & Design, 2022, 22 (4), pp.2181-2191. ⟨10.1021/acs.cgd.1c01246⟩
Journal articles hal-03619683v1
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Highly efficient polarizing agents for MAS‐DNP of proton‐dense molecular solids

Rania Harrabi , Thomas Halbritter , Fabien Aussenac , Ons Dakhlaoui , Johan van Tol
Angewandte Chemie International Edition, 2022, 61 (12), pp.e202114103. ⟨10.1002/anie.202114103⟩
Journal articles hal-03622904v1
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Targeted DNP for biomolecular solid-state NMR

Diego Gauto , Ons Dakhlaoui , Ildefonso Marin-Montesinos , Sabine Hediger , Gaël de Paëpe
Chemical Science, 2021, 12 (18), pp.6223-6237. ⟨10.1039/D0SC06959K⟩
Journal articles hal-03232087v1
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The surface chemistry of a nanocellulose drug carrier unravelled by MAS-DNP

Akshay Kumar , Hippolyte Durand , Elisa Zeno , Cyril Balsollier , Bastien Watbled
Chemical Science, 2020, 11 (15), pp.3868-3877. ⟨10.1039/C9SC06312A⟩
Journal articles hal-02566887v1
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Natural isotopic abundance $^{13}$C and $^{15}$N multidimensional solid-state NMR enabled by dynamic nuclear polarization

Adam Smith , Katharina Märker , Sabine Hediger , Gaël de Paëpe
Journal of Physical Chemistry Letters, 2019, 10 (16), pp.4652-4662. ⟨10.1021/acs.jpclett.8b03874⟩
Journal articles hal-02322267v1
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Selective high-resolution DNP-enhanced NMR of biomolecular binding sites

Ildefonso Marin-Montesinos , David Goyard , Emilie Gillon , Olivier Renaudet , Anne Imberty
Chemical Science, 2019, 10, pp.3366-3374. ⟨10.1039/c8sc05696j⟩
Journal articles hal-02052471v1
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De novo prediction of cross-effect efficiency for magic angle spinning dynamic nuclear polarization

Frederic Mentink Vigier , Anne-Laure Barra , Johan van Tol , Sabine Hediger , Daniel Lee
Physical Chemistry Chemical Physics, 2019, 21, pp.2166 - 2176. ⟨10.1039/C8CP06819D⟩
Journal articles hal-01981126v1
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Computationally Assisted Design of Polarizing Agents for Dynamic Nuclear Polarization Enhanced NMR: The AsymPol Family

Frederic Mentink-Vigier , Ildefonso Marin-Montesinos , Anil Jagtap , Thomas Halbritter , Johan van Tol
Journal of the American Chemical Society, 2018, 140 (35), pp.11013-11019. ⟨10.1021/jacs.8b04911⟩
Journal articles hal-02043262v1
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MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity

Sabine Hediger , Daniel Lee , Frederic Mentink-Vigier , Gaël de Paëpe
eMagRes, 2018, 7, pp.105-116. ⟨10.1002/9780470034590.emrstm1559⟩
Journal articles hal-02048719v1
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Structural Fingerprinting of Protein Aggregates by Dynamic Nuclear Polarization-Enhanced Solid-State NMR at Natural Isotopic Abundance

Adam Smith , Katharina Märker , Talia Piretra , Jennifer Boatz , Irina Matlahov
Journal of the American Chemical Society, 2018, 140 (44), pp.14576-14580. ⟨10.1021/jacs.8b09002⟩
Journal articles hal-02044496v1
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Welcoming natural isotopic abundance in solid-state NMR: probing π-stacking and supramolecular structure of organic nanoassemblies using DNP

Katharina Märker , Subhradip Paul , Carlos Fernandez-De-Alba , Daniel Lee , Jean-Marie Mouesca
Chemical Science, 2017, 8 (2), pp.974-987. ⟨10.1039/c6sc02709a⟩
Journal articles hal-02072153v1
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Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

Katharina Märker , Sabine Hediger , Gaël de Paëpe
Chemical Communications, 2017, 53 (65), pp.9155-9158. ⟨10.1039/C7CC04890D⟩
Journal articles hal-02048398v1
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Efficient cross-effect dynamic nuclear polarization without depolarization in high-resolution MAS NMR

Frederic Mentink-Vigier , Guinevere Mathies , Yangping Liu , Anne-Laure Barra , Marc A. Caporini
Chemical Science, 2017, 8 (12), pp.8150 - 8163. ⟨10.1039/c7sc02199b⟩
Journal articles hal-01667700v1

Ultra-low temperature MAS-DNP

Daniel Lee , Eric Bouleau , Pierre Saint-Bonnet , Sabine Hediger , Gael de Paepe
Journal of Magnetic Resonance, 2016, 264, pp.116-124. ⟨10.1016/j.jmr.2015.12.010⟩
Journal articles cea-01849839v1

Li-Rich Mn/Ni Layered Oxide as Electrode Material for Lithium Batteries: A Li-7 MAS NMR Study Revealing Segregation into (Nanoscale) Domains with Highly Different Electrochemical Behaviors

Anton Buzlukov , Jean-Marie Mouesca , Lucienne Buannic , Sabine Hediger , Loic Simonin
Journal of Physical Chemistry C, 2016, 120 (34), pp.19049-19063. ⟨10.1021/acs.jpcc.6b07532⟩
Journal articles cea-01849343v1

Li-Rich Mn/Ni Layered Oxide as Electrode Material for Lithium Batteries: A 7 Li MAS NMR Study Revealing Segregation into (Nanoscale) Domains with Highly Different Electrochemical Behaviors

Anton Buzlukov , Jean-Marie Mouesca , Lucienne Buannic , Sabine Hediger , Loïc Simonin
Journal of Physical Chemistry C, 2016, 120 (34), pp.19049-19063. ⟨10.1021/acs.jpcc.6b07532⟩
Journal articles hal-01939484v1

Pushing NMR sensitivity limits using dynamic nuclear polarization with closed-loop cryogenic helium sample spinning

Eric Bouleau , Pierre Saint-Bonnet , Frederic Mentink-Vigier , H. Takahashi , Jean-François Jacquot
Chemical Science, 2015, 6 (12), pp.6806-6812. ⟨10.1039/c5sc02819a⟩
Journal articles hal-01587521v1

Matrix-Free DNP-Enhanced NMR Spectroscopy of Liposomes Using a Lipid-Anchored Biradical

Carlos Fernandez-De-Alba , Hiroki Takahashi , Alexandre Richard , Yves Chenavier , Lionel Dubois
Chemistry - A European Journal, 2015, 21 (12), pp.4512-4517. ⟨10.1002/chem.201404588⟩
Journal articles hal-01592879v1

Is solid-state NMR enhanced by dynamic nuclear polarization?

Daniel Lee , Sabine Hediger , Gael de Paepe
Solid State Nuclear Magnetic Resonance, 2015, 66-67, pp.6-20. ⟨10.1016/j.ssnmr.2015.01.003⟩
Journal articles cea-01731479v1

Nuclear depolarization and absolute sensitivity in magic-angle spinning cross effect dynamic nuclear polarization

Frederic Mentink-Vigier , Subhradip Paul , Daniel Lee , Akiva Feintuch , Sabine Hediger
Physical Chemistry Chemical Physics, 2015, 17 (34), pp.21824-21836. ⟨10.1039/c5cp03457d⟩
Journal articles cea-01734609v1

A New Tool for NMR Crystallography: Complete C-13/N-15 Assignment of Organic Molecules at Natural Isotopic Abundance Using DNP-Enhanced Solid-State NMR

Katharina Marker , Morgane Pingret , Jean-Marie Mouesca , Didier Gasparutto , Sabine Hediger
Journal of the American Chemical Society, 2015, 137 (43), pp.13796-13799. ⟨10.1021/jacs.5b09964⟩
Journal articles cea-01734607v1

Third spin-assisted recoupling in SSNMR: theoretical insights and practicable application to biomolecular structure determination

Subhradip Paul , Hiroki Takahashi , Sabine Hediger , Gaël de Paëpe
Annual Reports on NMR Spectroscopy, 2015, 85, pp.93-142. ⟨10.1016/bs.arnmr.2014.12.003⟩
Journal articles hal-02052402v1
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Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments

Hiroki Takahashi , Carlos Fernandez-De-Alba , Daniel Lee , Vincent Maurel , Serge Gambarelli
Journal of Magnetic Resonance, 2014, 239, pp.91-99. ⟨10.1016/j.jmr.2013.12.005⟩
Journal articles hal-02043248v1

Windowed R-PDLF recoupling: a flexible and reliable tool to characterize molecular dynamics.

Axel Gansmüller , Jean-Pierre Simorre , Sabine Hediger
Journal of Magnetic Resonance, 2013, 234, pp.154-64. ⟨10.1016/j.jmr.2013.06.017⟩
Journal articles hal-01321571v1

Solid-state NMR on bacterial cells: selective cell wall signal enhancement and resolution improvement using dynamic nuclear polarization.

Hiroki Takahashi , Isabel Ayala , Michel Bardet , Gaël de Paëpe , Jean-Pierre Simorre
Journal of the American Chemical Society, 2013, 135 (13), pp.5105-10. ⟨10.1021/ja312501d⟩
Journal articles hal-01321585v1
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Rapid Natural-Abundance 2D 13 C- 13 C Correlation Spectroscopy Using Dynamic Nuclear Polarization Enhanced Solid-State NMR and Matrix-Free Sample Preparation

Hiroki Takahashi , Daniel Lee , Lionel Dubois , Michel Bardet , Sabine Hediger
Angewandte Chemie, 2012, 124 (47), pp.11936-11939. ⟨10.1002/anie.201206102⟩
Journal articles hal-02043242v1

NMR analysis of the transformation of wood constituents by torrefaction

T. Melkior , S. Jacob , G. Gerbaud , Sabine Hediger , L. Le Pape
Fuel, 2012, 92 (1), pp.271-280. ⟨10.1016/j.fuel.2011.06.042⟩
Journal articles hal-01233101v1

Structural characterization of metal–metal bonded polymer [Ru(L)(CO)2]n (L = 2,2′-bipyridine) in the solid state using high-resolution NMR and DFT chemical shift calculations

Guillaume Gerbaud , Jean-Marie Mouesca , Sabine Hediger , Sylvie Chardon-Noblat , Frédéric Lafolet
Physical Chemistry Chemical Physics, 2010, 12 (47), ⟨10.1039/c0cp00487a⟩
Journal articles hal-01658604v1

13C high-resolution solid-state NMR for structural elucidation of archaeological woods

M Bardet , G. Gerbaud , M. Giffard , C Doan , Sabine Hediger
Progress in Nuclear Magnetic Resonance Spectroscopy, 2009, 55 (3), pp.199-214. ⟨10.1016/j.pnmrs.2009.02.001⟩
Journal articles hal-01149630v1
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Nuclear magnetic resonance and electron paramagnetic resonance as analytical tools to investigate structural features of archaeological leathers

Michel Bardet , Guillaume Gerbaud , Laurent Le Pape , Sabine Hediger , Quôc-Khôc Trân
Analytical Chemistry, 2009, 81 (4), pp.1505-1511. ⟨10.1021/ac802052a⟩
Journal articles hal-01150976v1

Synthesis and solid-state NMR study of chromium complexes of per(3,6-anhydro)-α-cyclodextrin based polymers

Guillaume Gerbaud , Sabine Hediger , Andrée Gadelle , Michel Bardet
Carbohydrate Polymers, 2008, 73 (1), pp.64 - 73. ⟨10.1016/j.carbpol.2007.11.004⟩
Journal articles hal-01889742v1

Well-Defined Surface Tungstenocarbyne Complexes through the Reaction of [W(⋮C t Bu)(CH 2 t Bu) 3 ] with Silica

Erwan Le Roux , Mostafa Taoufik , Mathieu Chabanas , Damien Alcor , Anne Baudouin
Organometallics, 2005, 24 (17), pp.4274 - 4279. ⟨10.1021/om050086a⟩
Journal articles hal-01861682v1

Multi-dimensional magnetic resonance imaging in a stray magnetic field

Jay Baltisberger , Sabine Hediger , Lyndon Emsley
Journal of Magnetic Resonance, 2005, 172 (1), pp.79 - 84. ⟨10.1016/j.jmr.2004.09.019⟩
Journal articles hal-01906936v1
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Resolution Enhancement in Multidimensional Solid-State NMR Spectroscopy of Proteins using Spin-State Selection

Luminita Duma , Sabine Hediger , Bernhard Brutscher , Anja Böckmann , Lyndon Emsley
Journal of the American Chemical Society, 2003, 125, pp.11816. ⟨10.1021/ja036893n⟩
Journal articles hal-00078170v1

Resolution enhancement in multidimensional solid-state NMR spectroscopy of proteins using spin-state selection.

L. Duma , Sabine Hediger , B. Brutscher , A. Bockmann , L. Emsley
Journal of the American Chemical Society, 2003, 125, pp.11816-11817
Journal articles hal-00314370v1

Perhydrocarbyl Re VII Complexes: Comparison of Molecular and Surface Complexes

Mathieu Chabanas , Anne Baudouin , Christophe Copéret , Jean-Marie Basset , Wayne A Lukens
Journal of the American Chemical Society, 2003, 125 (2), pp.492 - 504. ⟨10.1021/ja020136s⟩
Journal articles hal-01702448v1
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High-Field Solid-State NMR with Dynamic Nuclear Polarization

Daniel Lee , Sabine Hediger , Gaël De Paëpe
Modern Magnetic Resonance 2017, Springer International Publishing, pp.1-17, 2017, ⟨10.1007/978-3-319-28275-6_73-1⟩
Book sections hal-02043260v1