Access content directly

Sabine Hediger

40
Documents

Publications

Image document

Fast magic angle spinning for the characterization of milligram quantities of organic and biological solids at natural isotopic abundance by 13C–13C correlation DNP-enhanced NMR

Adam Smith , Rania Harrabi , Thomas Halbritter , Daniel Lee , Fabien Aussenac
Solid State Nuclear Magnetic Resonance, 2023, 123, pp.101850. ⟨10.1016/j.ssnmr.2022.101850⟩
Journal articles hal-03927273v1
Image document

Optimizing chemistry at the surface of prodrug-loaded cellulose nanofibrils with MAS-DNP

Akshay Kumar , Bastien Watbled , Isabelle Baussanne , Sabine Hediger , Martine Demeunynck
Communications Chemistry, 2023, 6 (1), pp.58. ⟨10.1038/s42004-023-00852-2⟩
Journal articles hal-04049743v1
Image document

Biomolecular and Biological Applications of Solid-State NMR with Dynamic Nuclear Polarization Enhancement

Wing Ying Chow , Gaël de Paëpe , Sabine Hediger
Chemical Reviews, inPress, ⟨10.1021/acs.chemrev.1c01043⟩
Journal articles hal-03658826v1
Image document

Sonocrystallization of CMONS Needles and Nanocubes: Mechanistic Studies and Advanced Crystallinity Characterization by Combining X-ray and Electron Diffractions with DNP-Enhanced NMR

X. Cattoen , Akshay Kumar , Carole Vaillant , Mauricio Matta-Seclén , Fabien Dubois
Crystal Growth & Design, 2022, 22 (4), pp.2181-2191. ⟨10.1021/acs.cgd.1c01246⟩
Journal articles hal-03619683v1
Image document

Highly efficient polarizing agents for MAS‐DNP of proton‐dense molecular solids

Rania Harrabi , Thomas Halbritter , Fabien Aussenac , Ons Dakhlaoui , Johan van Tol
Angewandte Chemie International Edition, 2022, 61 (12), pp.e202114103. ⟨10.1002/anie.202114103⟩
Journal articles hal-03622904v1
Image document

Targeted DNP for biomolecular solid-state NMR

Diego Gauto , Ons Dakhlaoui , Ildefonso Marin-Montesinos , Sabine Hediger , Gaël de Paëpe
Chemical Science, 2021, 12 (18), pp.6223-6237. ⟨10.1039/D0SC06959K⟩
Journal articles hal-03232087v1
Image document

The surface chemistry of a nanocellulose drug carrier unravelled by MAS-DNP

Akshay Kumar , Hippolyte Durand , Elisa Zeno , Cyril Balsollier , Bastien Watbled
Chemical Science, 2020, 11 (15), pp.3868-3877. ⟨10.1039/C9SC06312A⟩
Journal articles hal-02566887v1
Image document

Natural isotopic abundance $^{13}$C and $^{15}$N multidimensional solid-state NMR enabled by dynamic nuclear polarization

Adam Smith , Katharina Märker , Sabine Hediger , Gaël de Paëpe
Journal of Physical Chemistry Letters, 2019, 10 (16), pp.4652-4662. ⟨10.1021/acs.jpclett.8b03874⟩
Journal articles hal-02322267v1
Image document

Selective high-resolution DNP-enhanced NMR of biomolecular binding sites

Ildefonso Marin-Montesinos , David Goyard , Emilie Gillon , Olivier Renaudet , Anne Imberty
Chemical Science, 2019, 10, pp.3366-3374. ⟨10.1039/c8sc05696j⟩
Journal articles hal-02052471v1
Image document

De novo prediction of cross-effect efficiency for magic angle spinning dynamic nuclear polarization

Frederic Mentink Vigier , Anne-Laure Barra , Johan van Tol , Sabine Hediger , Daniel Lee
Physical Chemistry Chemical Physics, 2019, 21, pp.2166 - 2176. ⟨10.1039/C8CP06819D⟩
Journal articles hal-01981126v1
Image document

Computationally Assisted Design of Polarizing Agents for Dynamic Nuclear Polarization Enhanced NMR: The AsymPol Family

Frederic Mentink-Vigier , Ildefonso Marin-Montesinos , Anil Jagtap , Thomas Halbritter , Johan van Tol
Journal of the American Chemical Society, 2018, 140 (35), pp.11013-11019. ⟨10.1021/jacs.8b04911⟩
Journal articles hal-02043262v1
Image document

MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity

Sabine Hediger , Daniel Lee , Frederic Mentink-Vigier , Gaël de Paëpe
eMagRes, 2018, 7, pp.105-116. ⟨10.1002/9780470034590.emrstm1559⟩
Journal articles hal-02048719v1
Image document

Structural Fingerprinting of Protein Aggregates by Dynamic Nuclear Polarization-Enhanced Solid-State NMR at Natural Isotopic Abundance

Adam Smith , Katharina Märker , Talia Piretra , Jennifer Boatz , Irina Matlahov
Journal of the American Chemical Society, 2018, 140 (44), pp.14576-14580. ⟨10.1021/jacs.8b09002⟩
Journal articles hal-02044496v1
Image document

Welcoming natural isotopic abundance in solid-state NMR: probing π-stacking and supramolecular structure of organic nanoassemblies using DNP

Katharina Märker , Subhradip Paul , Carlos Fernandez-De-Alba , Daniel Lee , Jean-Marie Mouesca
Chemical Science, 2017, 8 (2), pp.974-987. ⟨10.1039/c6sc02709a⟩
Journal articles hal-02072153v1
Image document

Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

Katharina Märker , Sabine Hediger , Gaël de Paëpe
Chemical Communications, 2017, 53 (65), pp.9155-9158. ⟨10.1039/C7CC04890D⟩
Journal articles hal-02048398v1
Image document

Efficient cross-effect dynamic nuclear polarization without depolarization in high-resolution MAS NMR

Frederic Mentink-Vigier , Guinevere Mathies , Yangping Liu , Anne-Laure Barra , Marc A. Caporini
Chemical Science, 2017, 8 (12), pp.8150 - 8163. ⟨10.1039/c7sc02199b⟩
Journal articles hal-01667700v1

Ultra-low temperature MAS-DNP

Daniel Lee , Eric Bouleau , Pierre Saint-Bonnet , Sabine Hediger , Gael de Paepe
Journal of Magnetic Resonance, 2016, 264, pp.116-124. ⟨10.1016/j.jmr.2015.12.010⟩
Journal articles cea-01849839v1

Li-Rich Mn/Ni Layered Oxide as Electrode Material for Lithium Batteries: A Li-7 MAS NMR Study Revealing Segregation into (Nanoscale) Domains with Highly Different Electrochemical Behaviors

Anton Buzlukov , Jean-Marie Mouesca , Lucienne Buannic , Sabine Hediger , Loic Simonin
Journal of Physical Chemistry C, 2016, 120 (34), pp.19049-19063. ⟨10.1021/acs.jpcc.6b07532⟩
Journal articles cea-01849343v1

Li-Rich Mn/Ni Layered Oxide as Electrode Material for Lithium Batteries: A 7 Li MAS NMR Study Revealing Segregation into (Nanoscale) Domains with Highly Different Electrochemical Behaviors

Anton Buzlukov , Jean-Marie Mouesca , Lucienne Buannic , Sabine Hediger , Loïc Simonin
Journal of Physical Chemistry C, 2016, 120 (34), pp.19049-19063. ⟨10.1021/acs.jpcc.6b07532⟩
Journal articles hal-01939484v1

Pushing NMR sensitivity limits using dynamic nuclear polarization with closed-loop cryogenic helium sample spinning

Eric Bouleau , Pierre Saint-Bonnet , Frederic Mentink-Vigier , H. Takahashi , Jean-François Jacquot
Chemical Science, 2015, 6 (12), pp.6806-6812. ⟨10.1039/c5sc02819a⟩
Journal articles hal-01587521v1

Matrix-Free DNP-Enhanced NMR Spectroscopy of Liposomes Using a Lipid-Anchored Biradical

Carlos Fernandez-De-Alba , Hiroki Takahashi , Alexandre Richard , Yves Chenavier , Lionel Dubois
Chemistry - A European Journal, 2015, 21 (12), pp.4512-4517. ⟨10.1002/chem.201404588⟩
Journal articles hal-01592879v1

Is solid-state NMR enhanced by dynamic nuclear polarization?

Daniel Lee , Sabine Hediger , Gael de Paepe
Solid State Nuclear Magnetic Resonance, 2015, 66-67, pp.6-20. ⟨10.1016/j.ssnmr.2015.01.003⟩
Journal articles cea-01731479v1

Nuclear depolarization and absolute sensitivity in magic-angle spinning cross effect dynamic nuclear polarization

Frederic Mentink-Vigier , Subhradip Paul , Daniel Lee , Akiva Feintuch , Sabine Hediger
Physical Chemistry Chemical Physics, 2015, 17 (34), pp.21824-21836. ⟨10.1039/c5cp03457d⟩
Journal articles cea-01734609v1

A New Tool for NMR Crystallography: Complete C-13/N-15 Assignment of Organic Molecules at Natural Isotopic Abundance Using DNP-Enhanced Solid-State NMR

Katharina Marker , Morgane Pingret , Jean-Marie Mouesca , Didier Gasparutto , Sabine Hediger
Journal of the American Chemical Society, 2015, 137 (43), pp.13796-13799. ⟨10.1021/jacs.5b09964⟩
Journal articles cea-01734607v1

Third spin-assisted recoupling in SSNMR: theoretical insights and practicable application to biomolecular structure determination

Subhradip Paul , Hiroki Takahashi , Sabine Hediger , Gaël de Paëpe
Annual Reports on NMR Spectroscopy, 2015, 85, pp.93-142. ⟨10.1016/bs.arnmr.2014.12.003⟩
Journal articles hal-02052402v1
Image document

Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments

Hiroki Takahashi , Carlos Fernandez-De-Alba , Daniel Lee , Vincent Maurel , Serge Gambarelli
Journal of Magnetic Resonance, 2014, 239, pp.91-99. ⟨10.1016/j.jmr.2013.12.005⟩
Journal articles hal-02043248v1

Windowed R-PDLF recoupling: a flexible and reliable tool to characterize molecular dynamics.

Axel Gansmüller , Jean-Pierre Simorre , Sabine Hediger
Journal of Magnetic Resonance, 2013, 234, pp.154-64. ⟨10.1016/j.jmr.2013.06.017⟩
Journal articles hal-01321571v1

Solid-state NMR on bacterial cells: selective cell wall signal enhancement and resolution improvement using dynamic nuclear polarization.

Hiroki Takahashi , Isabel Ayala , Michel Bardet , Gaël de Paëpe , Jean-Pierre Simorre
Journal of the American Chemical Society, 2013, 135 (13), pp.5105-10. ⟨10.1021/ja312501d⟩
Journal articles hal-01321585v1
Image document

Rapid Natural-Abundance 2D 13 C- 13 C Correlation Spectroscopy Using Dynamic Nuclear Polarization Enhanced Solid-State NMR and Matrix-Free Sample Preparation

Hiroki Takahashi , Daniel Lee , Lionel Dubois , Michel Bardet , Sabine Hediger
Angewandte Chemie, 2012, 124 (47), pp.11936-11939. ⟨10.1002/anie.201206102⟩
Journal articles hal-02043242v1

NMR analysis of the transformation of wood constituents by torrefaction

T. Melkior , S. Jacob , G. Gerbaud , Sabine Hediger , L. Le Pape
Fuel, 2012, 92 (1), pp.271-280. ⟨10.1016/j.fuel.2011.06.042⟩
Journal articles hal-01233101v1

Structural characterization of metal–metal bonded polymer [Ru(L)(CO)2]n (L = 2,2′-bipyridine) in the solid state using high-resolution NMR and DFT chemical shift calculations

Guillaume Gerbaud , Jean-Marie Mouesca , Sabine Hediger , Sylvie Chardon-Noblat , Frédéric Lafolet
Physical Chemistry Chemical Physics, 2010, 12 (47), ⟨10.1039/c0cp00487a⟩
Journal articles hal-01658604v1

13C high-resolution solid-state NMR for structural elucidation of archaeological woods

M Bardet , G. Gerbaud , M. Giffard , C Doan , Sabine Hediger
Progress in Nuclear Magnetic Resonance Spectroscopy, 2009, 55 (3), pp.199-214. ⟨10.1016/j.pnmrs.2009.02.001⟩
Journal articles hal-01149630v1
Image document

Nuclear magnetic resonance and electron paramagnetic resonance as analytical tools to investigate structural features of archaeological leathers

Michel Bardet , Guillaume Gerbaud , Laurent Le Pape , Sabine Hediger , Quôc-Khôc Trân
Analytical Chemistry, 2009, 81 (4), pp.1505-1511. ⟨10.1021/ac802052a⟩
Journal articles hal-01150976v1

Synthesis and solid-state NMR study of chromium complexes of per(3,6-anhydro)-α-cyclodextrin based polymers

Guillaume Gerbaud , Sabine Hediger , Andrée Gadelle , Michel Bardet
Carbohydrate Polymers, 2008, 73 (1), pp.64 - 73. ⟨10.1016/j.carbpol.2007.11.004⟩
Journal articles hal-01889742v1

Well-Defined Surface Tungstenocarbyne Complexes through the Reaction of [W(⋮C t Bu)(CH 2 t Bu) 3 ] with Silica

Erwan Le Roux , Mostafa Taoufik , Mathieu Chabanas , Damien Alcor , Anne Baudouin
Organometallics, 2005, 24 (17), pp.4274 - 4279. ⟨10.1021/om050086a⟩
Journal articles hal-01861682v1

Multi-dimensional magnetic resonance imaging in a stray magnetic field

Jay Baltisberger , Sabine Hediger , Lyndon Emsley
Journal of Magnetic Resonance, 2005, 172 (1), pp.79 - 84. ⟨10.1016/j.jmr.2004.09.019⟩
Journal articles hal-01906936v1
Image document

Resolution Enhancement in Multidimensional Solid-State NMR Spectroscopy of Proteins using Spin-State Selection

Luminita Duma , Sabine Hediger , Bernhard Brutscher , Anja Böckmann , Lyndon Emsley
Journal of the American Chemical Society, 2003, 125, pp.11816. ⟨10.1021/ja036893n⟩
Journal articles hal-00078170v1

Resolution enhancement in multidimensional solid-state NMR spectroscopy of proteins using spin-state selection.

L. Duma , Sabine Hediger , B. Brutscher , A. Bockmann , L. Emsley
Journal of the American Chemical Society, 2003, 125, pp.11816-11817
Journal articles hal-00314370v1

Perhydrocarbyl Re VII Complexes: Comparison of Molecular and Surface Complexes

Mathieu Chabanas , Anne Baudouin , Christophe Copéret , Jean-Marie Basset , Wayne A Lukens
Journal of the American Chemical Society, 2003, 125 (2), pp.492 - 504. ⟨10.1021/ja020136s⟩
Journal articles hal-01702448v1
Image document

High-Field Solid-State NMR with Dynamic Nuclear Polarization

Daniel Lee , Sabine Hediger , Gaël De Paëpe
Modern Magnetic Resonance 2017, Springer International Publishing, pp.1-17, 2017, ⟨10.1007/978-3-319-28275-6_73-1⟩
Book sections hal-02043260v1