Sabine Hediger

Publications

Article dans une revue (45)

Atomic Structure of Phosphorylated Nanocellulose Revealed by Dynamic Nuclear Polarization-Enhanced Solid-State NMR Tomohito Yagita,Subhradip Paul,Wassilios Papawassiliou,Akane Sakiyama,Yuka Tomitaet al. Journal of the American Chemical Society, 2026, 148 (4), pp.4237 - 4249. ⟨10.1021/jacs.5c17152⟩ Article dans une revue hal-05497889v1
Temperature-induced mobility in octacalcium phosphate impacts crystal symmetry: water dynamics studied by NMR crystallography Adam Nelson,Wassilios Papawassiliou,Subhradip Paul,Sabine Hediger,Ivan Hunget al. Faraday Discussions, 2025, 255, pp.451-482. ⟨10.1039/D4FD00108G⟩ Article dans une revue (data paper) hal-04930142v1
Artifact-free ultralow-temperature DNP-enhanced NMR of molecular assemblies at natural isotopic abundance Quentin Reynard-Feytis,Subhradip Paul,Sabine Hediger,Gaël de Paëpe Science Advances , 2025, 11 (51), ⟨10.1126/sciadv.aeb0337⟩ Article dans une revue hal-05442301v1
AsymPol-TEKs as efficient polarizing agents for MAS-DNP in glass matrices of non-aqueous solvents Rania Harrabi,Thomas Halbritter,Shadi Alarab,Satyaki Chatterjee,Malgorzata Wolska-Pietkiewiczet al. Physical Chemistry Chemical Physics, 2024, 26 (6), pp.5669-5682. ⟨10.1039/d3cp04271e⟩ Article dans une revue hal-04500679v1
PyrroTriPol: a semi-rigid trityl-nitroxide for high field dynamic nuclear polarization Thomas Halbritter,Rania Harrabi,Subhradip Paul,Johan van Tol,Daniel Leeet al. Chemical Science, 2023, 14 (14), pp.3852-3864. ⟨10.1039/d2sc05880d⟩ Article dans une revue hal-04234725v1
Optimizing chemistry at the surface of prodrug-loaded cellulose nanofibrils with MAS-DNP Akshay Kumar,Bastien Watbled,Isabelle Baussanne,Sabine Hediger,Martine Demeunyncket al. Communications Chemistry, 2023, 6 (1), pp.58. ⟨10.1038/s42004-023-00852-2⟩ Article dans une revue hal-04049743v1
Sustainable and cost-effective MAS DNP-NMR at 30 K with cryogenic sample exchange Subhradip Paul,Eric Bouleau,Quentin Reynard-Feytis,Jean-Pierre Arnaud,Florian Bancelet al. Journal of Magnetic Resonance, 2023, pp.107561. ⟨10.1016/j.jmr.2023.107561⟩ Article dans une revue hal-04234910v1
Fast magic angle spinning for the characterization of milligram quantities of organic and biological solids at natural isotopic abundance by 13C–13C correlation DNP-enhanced NMR Adam Smith,Rania Harrabi,Thomas Halbritter,Daniel Lee,Fabien Aussenacet al. Solid State Nuclear Magnetic Resonance, 2023, 123, pp.101850. ⟨10.1016/j.ssnmr.2022.101850⟩ Article dans une revue hal-03927273v1
Sonocrystallization of CMONS Needles and Nanocubes: Mechanistic Studies and Advanced Crystallinity Characterization by Combining X-ray and Electron Diffractions with DNP-Enhanced NMR X. Cattoen,Akshay Kumar,Carole Vaillant,Mauricio Matta-Seclén,Fabien Duboiset al. Crystal Growth & Design, 2022, 22 (4), pp.2181-2191. ⟨10.1021/acs.cgd.1c01246⟩ Article dans une revue hal-03619683v1
Highly efficient polarizing agents for MAS‐DNP of proton‐dense molecular solids Rania Harrabi,Thomas Halbritter,Fabien Aussenac,Ons Dakhlaoui,Johan van Tolet al. Angewandte Chemie International Edition, 2022, 61 (12), pp.e202114103. ⟨10.1002/anie.202114103⟩ Article dans une revue hal-03622904v1
Biomolecular and Biological Applications of Solid-State NMR with Dynamic Nuclear Polarization Enhancement Wing Ying Chow,Gaël de Paëpe,Sabine Hediger Chemical Reviews, 2022, 122 (10), pp.9795-9847. ⟨10.1021/acs.chemrev.1c01043⟩ Article dans une revue hal-03658826v1
Targeted DNP for biomolecular solid-state NMR Diego Gauto,Ons Dakhlaoui,Ildefonso Marin-Montesinos,Sabine Hediger,Gaël de Paëpe Chemical Science, 2021, 12 (18), pp.6223-6237. ⟨10.1039/D0SC06959K⟩ Article dans une revue hal-03232087v1
The surface chemistry of a nanocellulose drug carrier unravelled by MAS-DNP Akshay Kumar,Hippolyte Durand,Elisa Zeno,Cyril Balsollier,Bastien Watbledet al. Chemical Science, 2020, 11 (15), pp.3868-3877. ⟨10.1039/C9SC06312A⟩ Article dans une revue hal-02566887v1
Selective high-resolution DNP-enhanced NMR of biomolecular binding sites Ildefonso Marin-Montesinos,David Goyard,Emilie Gillon,Olivier Renaudet,Anne Imbertyet al. Chemical Science, 2019, 10, pp.3366-3374. ⟨10.1039/c8sc05696j⟩ Article dans une revue hal-02052471v1
Natural isotopic abundance $^{13}$C and $^{15}$N multidimensional solid-state NMR enabled by dynamic nuclear polarization Adam Smith,Katharina Märker,Sabine Hediger,Gaël de Paëpe Journal of Physical Chemistry Letters, 2019, 10 (16), pp.4652-4662. ⟨10.1021/acs.jpclett.8b03874⟩ Article dans une revue hal-02322267v1
De novo prediction of cross-effect efficiency for magic angle spinning dynamic nuclear polarization Frederic Mentink Vigier,Anne-Laure Barra,Johan van Tol,Sabine Hediger,Daniel Leeet al. Physical Chemistry Chemical Physics, 2019, 21, pp.2166 - 2176. ⟨10.1039/C8CP06819D⟩ Article dans une revue hal-01981126v1
MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity Sabine Hediger,Daniel Lee,Frederic Mentink-Vigier,Gaël de Paëpe eMagRes, 2018, 7, pp.105-116. ⟨10.1002/9780470034590.emrstm1559⟩ Article dans une revue hal-02048719v1
Computationally Assisted Design of Polarizing Agents for Dynamic Nuclear Polarization Enhanced NMR: The AsymPol Family Frederic Mentink-Vigier,Ildefonso Marin-Montesinos,Anil Jagtap,Thomas Halbritter,Johan van Tolet al. Journal of the American Chemical Society, 2018, 140 (35), pp.11013-11019. ⟨10.1021/jacs.8b04911⟩ Article dans une revue hal-02043262v1
Structural Fingerprinting of Protein Aggregates by Dynamic Nuclear Polarization-Enhanced Solid-State NMR at Natural Isotopic Abundance Adam Smith,Katharina Märker,Talia Piretra,Jennifer Boatz,Irina Matlahovet al. Journal of the American Chemical Society, 2018, 140 (44), pp.14576-14580. ⟨10.1021/jacs.8b09002⟩ Article dans une revue hal-02044496v1
Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths Katharina Märker,Sabine Hediger,Gaël de Paëpe Chemical Communications, 2017, 53 (65), pp.9155-9158. ⟨10.1039/C7CC04890D⟩ Article dans une revue hal-02048398v1
Welcoming natural isotopic abundance in solid-state NMR: probing π-stacking and supramolecular structure of organic nanoassemblies using DNP Katharina Märker,Subhradip Paul,Carlos Fernandez-De-Alba,Daniel Lee,Jean-Marie Mouescaet al. Chemical Science, 2017, 8 (2), pp.974-987. ⟨10.1039/c6sc02709a⟩ Article dans une revue hal-02072153v1
Efficient cross-effect dynamic nuclear polarization without depolarization in high-resolution MAS NMR Frederic Mentink-Vigier,Guinevere Mathies,Yangping Liu,Anne-Laure Barra,Marc A. Caporiniet al. Chemical Science, 2017, 8 (12), pp.8150 - 8163. ⟨10.1039/c7sc02199b⟩ Article dans une revue hal-01667700v1
Ultra-low temperature MAS-DNP Daniel Lee,Eric Bouleau,Pierre Saint-Bonnet,Sabine Hediger,Gael de Paepe Journal of Magnetic Resonance, 2016, 264, pp.116-124. ⟨10.1016/j.jmr.2015.12.010⟩ Article dans une revue istex cea-01849839v1
Li-Rich Mn/Ni Layered Oxide as Electrode Material for Lithium Batteries: A Li-7 MAS NMR Study Revealing Segregation into (Nanoscale) Domains with Highly Different Electrochemical Behaviors Anton Buzlukov,Jean-Marie Mouesca,Lucienne Buannic,Sabine Hediger,Loic Simoninet al. Journal of Physical Chemistry C, 2016, 120 (34), pp.19049-19063. ⟨10.1021/acs.jpcc.6b07532⟩ Article dans une revue cea-01849343v1
Li-Rich Mn/Ni Layered Oxide as Electrode Material for Lithium Batteries: A 7 Li MAS NMR Study Revealing Segregation into (Nanoscale) Domains with Highly Different Electrochemical Behaviors Anton Buzlukov,Jean-Marie Mouesca,Lucienne Buannic,Sabine Hediger,Loïc Simoninet al. Journal of Physical Chemistry C, 2016, 120 (34), pp.19049-19063. ⟨10.1021/acs.jpcc.6b07532⟩ Article dans une revue hal-01939484v1
Is solid-state NMR enhanced by dynamic nuclear polarization? Daniel Lee,Sabine Hediger,Gael de Paepe Solid State Nuclear Magnetic Resonance, 2015, 66-67, pp.6-20. ⟨10.1016/j.ssnmr.2015.01.003⟩ Article dans une revue istex cea-01731479v1
Pushing NMR sensitivity limits using dynamic nuclear polarization with closed-loop cryogenic helium sample spinning Eric Bouleau,Pierre Saint-Bonnet,Frederic Mentink-Vigier,H. Takahashi,Jean-François Jacquotet al. Chemical Science, 2015, 6 (12), pp.6806-6812. ⟨10.1039/c5sc02819a⟩ Article dans une revue hal-01587521v1
Nuclear depolarization and absolute sensitivity in magic-angle spinning cross effect dynamic nuclear polarization Frederic Mentink-Vigier,Subhradip Paul,Daniel Lee,Akiva Feintuch,Sabine Hedigeret al. Physical Chemistry Chemical Physics, 2015, 17 (34), pp.21824-21836. ⟨10.1039/c5cp03457d⟩ Article dans une revue cea-01734609v1
Matrix-Free DNP-Enhanced NMR Spectroscopy of Liposomes Using a Lipid-Anchored Biradical Carlos Fernandez-De-Alba,Hiroki Takahashi,Alexandre Richard,Yves Chenavier,Lionel Duboiset al. Chemistry - A European Journal, 2015, 21 (12), pp.4512-4517. ⟨10.1002/chem.201404588⟩ Article dans une revue istex hal-01592879v1
A New Tool for NMR Crystallography: Complete C-13/N-15 Assignment of Organic Molecules at Natural Isotopic Abundance Using DNP-Enhanced Solid-State NMR Katharina Marker,Morgane Pingret,Jean-Marie Mouesca,Didier Gasparutto,Sabine Hedigeret al. Journal of the American Chemical Society, 2015, 137 (43), pp.13796-13799. ⟨10.1021/jacs.5b09964⟩ Article dans une revue cea-01734607v1
Third spin-assisted recoupling in SSNMR: theoretical insights and practicable application to biomolecular structure determination Subhradip Paul,Hiroki Takahashi,Sabine Hediger,Gaël de Paëpe Annual Reports on NMR Spectroscopy, 2015, 85, pp.93-142. ⟨10.1016/bs.arnmr.2014.12.003⟩ Article dans une revue hal-02052402v1
Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments Hiroki Takahashi,Carlos Fernandez-De-Alba,Daniel Lee,Vincent Maurel,Serge Gambarelliet al. Journal of Magnetic Resonance, 2014, 239, pp.91-99. ⟨10.1016/j.jmr.2013.12.005⟩ Article dans une revue hal-02043248v1
Windowed R-PDLF recoupling: a flexible and reliable tool to characterize molecular dynamics. Axel Gansmüller,Jean-Pierre Simorre,Sabine Hediger Journal of Magnetic Resonance, 2013, 234, pp.154-64. ⟨10.1016/j.jmr.2013.06.017⟩ Article dans une revue istex hal-01321571v1
Solid-state NMR on bacterial cells: selective cell wall signal enhancement and resolution improvement using dynamic nuclear polarization. Hiroki Takahashi,Isabel Ayala,Michel Bardet,Gaël de Paëpe,Jean-Pierre Simorreet al. Journal of the American Chemical Society, 2013, 135 (13), pp.5105-10. ⟨10.1021/ja312501d⟩ Article dans une revue hal-01321585v1
Rapid Natural-Abundance 2D 13 C- 13 C Correlation Spectroscopy Using Dynamic Nuclear Polarization Enhanced Solid-State NMR and Matrix-Free Sample Preparation Hiroki Takahashi,Daniel Lee,Lionel Dubois,Michel Bardet,Sabine Hedigeret al. Angewandte Chemie, 2012, 124 (47), pp.11936-11939. ⟨10.1002/anie.201206102⟩ Article dans une revue istex hal-02043242v1
NMR analysis of the transformation of wood constituents by torrefaction T. Melkior,S. Jacob,G. Gerbaud,Sabine Hediger,L. Le Papeet al. Fuel, 2012, 92 (1), pp.271-280. ⟨10.1016/j.fuel.2011.06.042⟩ Article dans une revue istex hal-01233101v1
Structural characterization of metal–metal bonded polymer [Ru(L)(CO)2]n (L = 2,2′-bipyridine) in the solid state using high-resolution NMR and DFT chemical shift calculations Guillaume Gerbaud,Jean-Marie Mouesca,Sabine Hediger,Sylvie Chardon-Noblat,Frédéric Lafoletet al. Physical Chemistry Chemical Physics, 2010, 12 (47), ⟨10.1039/c0cp00487a⟩ Article dans une revue istex hal-01658604v1
13C high-resolution solid-state NMR for structural elucidation of archaeological woods M Bardet,G. Gerbaud,M. Giffard,C Doan,Sabine Hedigeret al. Progress in Nuclear Magnetic Resonance Spectroscopy, 2009, 55 (3), pp.199-214. ⟨10.1016/j.pnmrs.2009.02.001⟩ Article dans une revue istex hal-01149630v1
Nuclear magnetic resonance and electron paramagnetic resonance as analytical tools to investigate structural features of archaeological leathers Michel Bardet,Guillaume Gerbaud,Laurent Le Pape,Sabine Hediger,Quôc-Khôc Trânet al. Analytical Chemistry, 2009, 81 (4), pp.1505-1511. ⟨10.1021/ac802052a⟩ Article dans une revue hal-01150976v1
Synthesis and solid-state NMR study of chromium complexes of per(3,6-anhydro)-α-cyclodextrin based polymers Guillaume Gerbaud,Sabine Hediger,Andrée Gadelle,Michel Bardet Carbohydrate Polymers, 2008, 73 (1), pp.64 - 73. ⟨10.1016/j.carbpol.2007.11.004⟩ Article dans une revue istex hal-01889742v1
Well-Defined Surface Tungstenocarbyne Complexes through the Reaction of [W(⋮C t Bu)(CH 2 t Bu) 3 ] with Silica Erwan Le Roux,Mostafa Taoufik,Mathieu Chabanas,Damien Alcor,Anne Baudouinet al. Organometallics, 2005, 24 (17), pp.4274 - 4279. ⟨10.1021/om050086a⟩ Article dans une revue istex hal-01861682v1
Multi-dimensional magnetic resonance imaging in a stray magnetic field Jay Baltisberger,Sabine Hediger,Lyndon Emsley Journal of Magnetic Resonance, 2005, 172 (1), pp.79 - 84. ⟨10.1016/j.jmr.2004.09.019⟩ Article dans une revue istex hal-01906936v1
Perhydrocarbyl Re VII Complexes: Comparison of Molecular and Surface Complexes Mathieu Chabanas,Anne Baudouin,Christophe Copéret,Jean-Marie Basset,Wayne A Lukenset al. Journal of the American Chemical Society, 2003, 125 (2), pp.492 - 504. ⟨10.1021/ja020136s⟩ Article dans une revue istex hal-01702448v1
Resolution enhancement in multidimensional solid-state NMR spectroscopy of proteins using spin-state selection. L. Duma,Sabine Hediger,B. Brutscher,A. Bockmann,L. Emsley Journal of the American Chemical Society, 2003, 125, pp.11816-11817 Article dans une revue hal-00314370v1
Resolution Enhancement in Multidimensional Solid-State NMR Spectroscopy of Proteins using Spin-State Selection Luminita Duma,Sabine Hediger,Bernhard Brutscher,Anja Böckmann,Lyndon Emsley Journal of the American Chemical Society, 2003, 125, pp.11816. ⟨10.1021/ja036893n⟩ Article dans une revue hal-00078170v1

Communication dans un congrès (1)

La DNP-RMN haute résolution à basse température en autonomie fluidique Eric Bouleau,Gaël de Paëpe,Florian Bancel,Bertrand Rollet,Clarisse Bourbonet al. 13èmes journées de Cryogénie et supraconductivité, AFFCCS, Oct 2021, Aussois (FR), France Communication dans un congrès hal-04908839v1

Chapitre d'ouvrage (1)

High-Field Solid-State NMR with Dynamic Nuclear Polarization Daniel Lee,Sabine Hediger,Gaël De Paëpe Modern Magnetic Resonance 2017, Springer International Publishing, pp.1-17, 2017, ⟨10.1007/978-3-319-28275-6_73-1⟩ Chapitre d'ouvrage hal-02043260v1

Pré-publication, Document de travail (1)

Removing t1-noise in DNP-enhanced NMR at natural isotopic abundance using two-spin order filter Quentin Reynard--Feytis,Subhradip Paul,Sabine Hediger,Gaël de Paëpe 2025 Pré-publication, Document de travail (preprint/prepublication) hal-05344475v1