Philippe Lesot

152
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Publications

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Development of Deep Learning Software to Improve HPLC and GC Predictions using a new Crown-ether based Mesogenic Stationary Phase and Beyond

Warda Fella Belaid , Azeddine Dekhira , Philippe Lesot , Ouassila Ferroukhi
Journal of Chromatography A, 2025, 1739, pp.465476. ⟨10.1016/j.chroma.2024.465476⟩
Article dans une revue hal-04799963 v1
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Potential and Performance of Anisotropic 19F NMR for the Enantiomeric Analysis of Fluorinated Chiral Active Pharmaceutical Ingredients

Boris Gouilleux , François-Marie Moussallieh , Philippe Lesot
Analyst, In press, 149, pp.3204-3213. ⟨10.1039/d4an00237g⟩
Article dans une revue hal-04558310 v1
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Spatially Resolved Anisotropic Natural Abundance Deuterium 2D-NMR Spectroscopy Using Bimesophasic Lyotropic Chiral Systems

Thomas Julien , Boris Gouilleux , Bernard Rousseau , Stefan Immel , Michael Reggelin et al.
Journal of Physical Chemistry Letters, 2024, 15 (7), pp.2089-2095. ⟨10.1021/acs.jpclett.3c03302⟩
Article dans une revue hal-04471708 v1
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Anisotropic 1H STD‐NMR Spectroscopy: Exploration of Enantiomer‐Polypeptide Interactions in Chiral Oriented Environments

Boris Gouilleux , Francois-Marie Moussallieh , Philippe Lesot
ChemPhysChem, 2022, 24 (4), pp.e202200508. ⟨10.1002/cphc.202200508⟩
Article dans une revue hal-03800520 v1
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Study and quantification of enantiodiscrimination power of four polymeric chiral LLCs using NAD 2D-NMR

Philippe Berdagué , Boris Gouilleux , Markus Noll , Stefan Immel , Michael Reggelin et al.
Physical Chemistry Chemical Physics, 2022, 24 (12), pp.7338-7348. ⟨10.1039/D1CP04915A⟩
Article dans une revue hal-03586878 v1
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Molecular enantiodiscrimination by NMR spectroscopy in chiral oriented systems: Concept, tools, and applications

Christie Aroulanda , Philippe Lesot
Chirality, 2022, 34, pp.182-244. ⟨10.1002/chir.23386⟩
Article dans une revue hal-03512385 v1
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Exploring the enantiomeric 13C position-specific isotope fractionation: challenges and anisotropic NMR-based analytical strategy

Philippe Lesot , Philippe Berdagué , Virginie Silvestre , Gérald Remaud
Analytical and Bioanalytical Chemistry, 2021, 413 (25), pp.6379-6392. ⟨10.1007/s00216-021-03599-8⟩
Article dans une revue hal-03409628 v1
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Deuterium Residual Quadrupolar Couplings: Crossing the Current Frontiers in the Relative Configuration Analysis of Natural Products

Philippe Lesot , Roberto R. Gil , Philippe Berdague , Armando Navarro-Vázquez
Journal of Natural Products, 2020, 83 (10), pp.3141-3148. ⟨10.1021/acs.jnatprod.0c00745⟩
Article dans une revue hal-02949550 v1
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Hydrogen isotope exchange catalyzed by Ru nanocatalysts: labelling of complex molecules containing N-heterocycles and reaction mechanism insights

Viktor Pfeifer , Marie Certiat , Donia Bouzouita , Alberto Palazzolo , Sébastien Garcia-Argote et al.
Chemistry - A European Journal, 2020, 26, pp.4988-4996. ⟨10.1002/chem.201905651⟩
Article dans une revue cea-02487414 v1
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Tuning the Reactivity of a Heterogeneous Catalyst using N‐Heterocyclic Carbene Ligands for C−H Activation Reactions

Alberto Palazzolo , Timothée Naret , Marion Daniel‐bertrand , David‐alexandre Buisson , Simon Tricard et al.
Angewandte Chemie International Edition, 2020, 59 (47), pp.20879-20884. ⟨10.1002/anie.202009258⟩
Article dans une revue hal-03001484 v1
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Chemical Synthesis of [ 2 H]-Ethyl Tosylate and Exploration of Its Crypto-optically Active Character Combining Complementary Spectroscopic Tools

Timothée Naret , Philippe Lesot , Andrew Puente , Prasad Polavarapu , David-Alexandre Buisson et al.
Organic Letters, 2020, 22 (22), pp.8846-8849. ⟨10.1021/acs.orglett.0c03219⟩
Article dans une revue hal-02987518 v2
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2H QUOSY 2D-NMR Experiments in Weakly Aligning Systems: From the Conventional to the UF Approach

Boris Gouilleux , Abdelkrim Meddour , Philippe Lesot
ChemPhysChem, 2020, 21, pp.1548-1563. ⟨10.1002/cphc.202000336⟩
Article dans une revue hal-02623845 v1
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Determination of the natural deuterium distribution of fatty acids by application of 2H 2D-NMR in liquid crystals: fundamentals, advances, around and beyond

Philippe Lesot
Liquid Crystals, 2020, 47 (13), pp.1889-1910. ⟨10.1080/02678292.2019.1613685⟩
Article dans une revue hal-02308723 v1
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2H and 13C NMR-Based Enantiodetection Using Polyacetylene versus Polypeptide Aligning Media: Versatile and Complementary Tools for Chemists

Philippe Lesot , Philippe Berdagué , Abdelkrim Meddour , Alexander Kreiter , Markus Noll et al.
ChemPlusChem, 2019, 84 (2), pp.144-153. ⟨10.1002/cplu.201800493⟩
Article dans une revue hal-02308749 v1

(Cover Profile) 2H and 13C NMR-Based Enantiodetection Using Polyacetylene versus Polypeptide Aligning Media: Versatile and Complementary Tools for Chemists

Philippe Lesot , Philippe Berdagué , Abdelkrim Meddour , Alexander Kreiter , Markus Noll et al.
ChemPlusChem, 2019, pp.143-143. ⟨10.1002/cplu.201800584⟩
Article dans une revue hal-02308742 v1
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Designing and building a low-cost portable FT-NMR spectrometer in 2019: A modern challenge

Alain Louis-Joseph , Philippe Lesot
Comptes Rendus. Chimie, 2019, 22, pp.695-711. ⟨10.1016/j.crci.2019.07.001⟩
Article dans une revue hal-02308789 v1
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Multinuclear NMR in Polypeptide Liquid Crystals: Three Fertile Decades of Methodological Developments and Analytical Challenges

Philippe Lesot , Christie Aroulanda , Philippe Berdagué , Abdelkrim Meddour , Denis Merlet et al.
Progress in Nuclear Magnetic Resonance Spectroscopy, 2019, Progress in Nuclear Magnetic Resonance Spectroscopy, 116, pp.85-154. ⟨10.1016/j.pnmrs.2019.10.001⟩
Article dans une revue hal-02351278 v1

Ruthenium-catalyzed hydrogen isotope exchange of C(sp3)–H bonds directed by a sulfur atom

Longhui Gao , Serge Perato , Sébastien Garcia-Argote , Céline Taglang , Luis Miguel Martinez-Pietro et al.
Chemical Communications, 2018, 54 (24), pp.2986-2989. ⟨10.1039/C8CC00653A⟩
Article dans une revue hal-02308831 v1

Analytical contribution of deuterium 2D-NMR in oriented media to H-2/H-1 isotopic characterization: the case of vanillin

Tristan Texier-Bonniot , Philippe Berdague , Richard J. Robins , Gérald Remaud , Philippe Lesot
Flavour and Fragrance Journal, 2018, 33 (3), pp.217-229. ⟨10.1002/ffj.3441⟩
Article dans une revue hal-02140951 v1

À MRFood 2018, les sciences slimentaires rencontrent la spectroscopie par résonance magnétique!

Philippe Lesot
Spectra Analyse, 2018, 323, pp.18-20
Article dans une revue hal-02317627 v1

La “39th FGMR Annual Discussion Meeting 2017”: La Spectroscopie Magnétique Franco-Allemande dans tous ses “Etats”!

Philippe Lesot
Spectra Analyse, 2017, pp.12-14
Article dans une revue hal-02317591 v1

RMN de Paillasse à Transformée de Fourier: Le Renouveau de la RMN à Bas Champ.

Philippe Lesot
Spectra Analyse, 2017, 315, pp.32-62
Article dans une revue hal-02317538 v1

Integrated Computational Protocol for the Analysis of Quadrupolar Splittings from Natural-Abundance Deuterium NMR Spectra in (Chiral) Oriented Media

Armando Navarro-Vázquez , Philippe Berdagué , Philippe Lesot
ChemPhysChem, 2017, 18 (10), pp.1252-1266. ⟨10.1002/cphc.201601423⟩
Article dans une revue hal-02308835 v1

(Cover profile) Integrated Computational Protocol for the Analysis of Quadrupolar Splittings from Natural-Abundance Deuterium NMR Spectra in (Chiral) Oriented Media

Armando Navarro-Vázquez , Philippe Berdagué , Philippe Lesot
ChemPhysChem, 2017, pp.1219-1219. ⟨10.1002/CPHC.201700454⟩
Article dans une revue hal-02308843 v1
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Contribution of NAD 2D-NMR in liquid crystals to the determination of hydrogen isotope profile of methyl groups in miliacin

Philippe Berdagué , Philippe Lesot , Jérémy Jacob , Valery T. Terwilliger , Claude Le Milbeau
Geochimica et Cosmochimica Acta, 2016, 173, pp.337-351. ⟨10.1016/j.gca.2015.10.004⟩
Article dans une revue insu-01225227 v1

Investigation of Solute-Fiber Affinity and Orientational Ordering of Norbornadiene Interacting with Two-Polypeptide Chiral Liquid Crystalline Solvents by Natural Abundance Deuterium (NAD) NMR

Zeinab Serhan , Christie Aroulanda , Philippe Lesot
Journal of Physical Chemistry A, 2016, 120 (30), pp.6076-6088. ⟨10.1021/acs.jpca.6b04254⟩
Article dans une revue hal-03004599 v1
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Detection of quadrupolar nuclei by ultrafast 2D NMR: exploring the case of deuterated analytes aligned in chiral oriented solvents

Philippe Lesot , Philippe Berdagué , Patrick Giraudeau
Chemical Communications, 2016, 52 (10), pp.2122-2125. ⟨10.1039/C5CC09409G⟩
Article dans une revue hal-02314360 v1

Fast acquisition of multidimensional NMR spectra of solids and mesophases using alternative sampling methods

Philippe Lesot , Krzysztof Kazimierczuk , Julien Trébosc , Jean-Paul Amoureux , Olivier Lafon
Magnetic Resonance in Chemistry, 2015, 53 (11), pp.927-939. ⟨10.1002/mrc.4290⟩
Article dans une revue istex hal-02314353 v1

Enantiotopic discrimination in the NMR spectrum of prochiral solutes in chiral liquid crystals

Philippe Lesot , Christie Aroulanda , Herbert Zimmermann , Zeev Luz
Chemical Society Reviews, 2015, 44 (8), pp.2330-2375
Article dans une revue hal-02314352 v1

Vladimir I. Bakhmutov: NMR spectroscopy in liquids and solids

Philippe Lesot
Analytical and Bioanalytical Chemistry, 2015, 407 (29), pp.8625-8626. ⟨10.1007/s00216-015-9061-z⟩
Article dans une revue hal-02314356 v1

Chronique Littéraire: « NMR Spectroscopy in Liquid and Solids » de V. I. Bakhmutov

Philippe Lesot
Spectra Analyse, 2015, 306, pp.16-16
Article dans une revue hal-02317530 v1

Synthesis and Stereochemical Assignment of Crypto-Optically Active 2-H6 -Neopentane

Ahmad Masarwa , Dennis Gerbig , Liron Oskar , Aharon Loewenstein , Hans Peter Reisenauer et al.
Angewandte Chemie International Edition, 2015, 54 (44), pp.13106-13109. ⟨10.1002/anie.201505349⟩
Article dans une revue istex hal-03010704 v1

Synthese und stereochemische Bestimmung von krypto-optisch-aktivem 2H6 -Neopentan

Ahmad Masarwa , Dennis Gerbig , Liron Oskar , Aharon Loewenstein , Hans Peter Reisenauer et al.
Angewandte Chemie, 2015, 127 (44), pp.13298-13302. ⟨10.1002/ange.201505349⟩
Article dans une revue istex hal-02314354 v1

Multi-nuclear NMR of axially chiral biaryls in polypeptide orienting solvents: spectral discriminations and enantiorecognition mechanisms

Philippe Berdagué , Jose-Enrique Herbert-Pucheta , Vishwajeet Jha , Armen Panossian , Frédéric Leroux et al.
New Journal of Chemistry, 2015, 39 (12), pp.9504-9517. ⟨10.1039/c5nj01434d⟩
Article dans une revue hal-02314357 v1

Correlation 2D-NMR experiments involving both $^{13}$C and $^{2}$H isotopes in oriented media: methodological developments and analytical applications

Philippe Lesot , Olivier Lafon , Philippe Berdagué
Magnetic Resonance in Chemistry, 2014, 52 (10), pp.595-613. ⟨10.1002/mrc.4118⟩
Article dans une revue istex hal-02314351 v1

NMR discrimination in nonrigid prochiral solutes dissolved in chiral liquid crystals: symmetry considerations

Philippe Lesot , Zeev Luz , Christie Aroulanda , Herbert Zimmermann
Magnetic Resonance in Chemistry, 2014, 52 (10), pp.581-594. ⟨10.1002/mrc.4110⟩
Article dans une revue istex hal-02314350 v1

RMN 2D DAN dans les CLC: de nouveaux outils pour l’étude du fractionnement isotopique naturel (2H/1H) d’acides gras et de triglycérides

Philippe Lesot
Spectra Analyse, 2014, 299 (62-72)
Article dans une revue hal-02317515 v1

Criteria for sensitivity enhancement by compressed sensing: practical application to anisotropic NAD 2D-NMR spectroscopy

Krzysztof Kazimierczuk , Olivier Lafon , Philippe Lesot
Analyst, 2014, 139 (11), pp.2702. ⟨10.1039/c4an00381k⟩
Article dans une revue hal-02314349 v1

Synthesis of a Mycobacterium tuberculosis tetra-acylated sulfolipid analogue and characterization of the chiral acyl chains using anisotropic NAD 2D-NMR spectroscopy.

Aurélie Lemétais , Yann Bourdreux , Philippe Lesot , Jonathan Farjon , Jean-Marie Beau
Journal of Organic Chemistry, 2013, 78 (15), pp.7648-57. ⟨10.1021/jo4012255⟩
Article dans une revue hal-00910978 v1

Chiral solutes can seed the formation of enantiomorphic domains in a twist-bend nematic liquid crystal

James Emsley , Philippe Lesot , Geoffrey Luckhurst , Abdelkrim Meddour , Denis Merlet
Physical Review E : Statistical, Nonlinear, and Soft Matter Physics, 2013, 87 (4), ⟨10.1103/PhysRevE.87.040501⟩
Article dans une revue hal-02311510 v1

Multiscale NMR investigation of mesogenic ionic-liquid electrolytes with strong anisotropic orientational and diffusional behaviour

Patrick Judeinstein , Stéphanie Huet , Philippe Lesot
RSC Advances, 2013, 3 (37), pp.16604. ⟨10.1039/C3RA00025G⟩
Article dans une revue hal-02311512 v1

On-the-fly' Kinetics of Enzymatic Racemization using Deuterium NMR in DNA-based Chiral Oriented Media.

Monique Chan-Huot , Philippe Georges Julien Lesot , Philippe Pelupessy , Luminita Duma , Geoffrey Bodenhausen et al.
Analytical Chemistry, 2013, 85 (9), pp.4694-4697. ⟨10.1021/ac4004002⟩
Article dans une revue hal-00807811 v1

Synthesis of enones, pyrazolines and pyrrolines with gem-difluoroalkyl side chains

Assaad Nasr El Dine , Ali Khalaf , Danielle Gree , Olivier Tasseau , Fares Fares et al.
Beilstein Journal of Organic Chemistry, 2013, 9, pp.1943-1948. ⟨10.3762/bjoc.9.230⟩
Article dans une revue hal-00871797 v1

Probing substrate-product relationships by natural abundance deuterium 2D NMR spectroscopy in liquid-crystalline solvents: epoxidation of linoleate to vernoleate by two different plant enzymes

Isabelle Billault , Alicia Le Du , Minale Ouethrani , Zeinab Serhan , Philippe Lesot et al.
Analytical and Bioanalytical Chemistry, 2012, 402 (9), pp.2985-2998. ⟨10.1007/s00216-012-5748-6⟩
Article dans une revue istex hal-02142700 v1

Is Enantiomer Assignment Possible by NMR Spectroscopy Using Residual Dipolar Couplings from Chiral Nonracemic Alignment Media?-A Critical Assessment

Robert Berger , Jacques Courtieu , Roberto Gil , Christian Griesinger , Matthias Köck et al.
Angewandte Chemie International Edition, 2012, 51 (33), pp.8388-8391. ⟨10.1002/anie.201107626⟩
Article dans une revue istex hal-02311507 v1

Analysis of NAD 2D-NMR Spectra of Saturated Fatty Acids in Polypeptide Aligning Media by Experimental and Modeling Approaches

Zeinab Serhan , Andrea Borgogno , Isabelle Billault , Alberta Ferrarini , Philippe Lesot
Chemistry - A European Journal, 2012, 18 (1), pp.117-126. ⟨10.1002/chem.201102775⟩
Article dans une revue istex hal-02143143 v1

Inside Cover: Analysis of NAD 2D-NMR Spectra of Saturated Fatty Acids in Polypeptide Aligning Media by Experimental and Modeling Approaches (Chem. Eur. J. 1/2012)

Zeinab Serhan , Andrea Borgogno , Isabelle Billault , Alberta Ferrarini , Philippe Lesot
Chemistry - A European Journal, 2012, 18 (1), pp.2-2. ⟨10.1002/chem.201190273⟩
Article dans une revue hal-02316063 v1

Experimental Detection of Achiral and Chiral Naturally Abundant 13 C– 2 H Isotopomers by 2D-NMR in Liquids and Chiral Oriented Solvents

Philippe Lesot , Olivier Lafon
Analytical Chemistry, 2012, 84 (10), pp.4569-4573. ⟨10.1021/ac300667n⟩
Article dans une revue hal-02311506 v1

La RMN en chimie organique

Jacques Courtieu , Nicolas Giraud , Olivier Lafon , Philippe Lesot , Jean-Marc Nuzillard et al.
L'Actualité Chimique, 2012, 364-365, pp.30-41
Article dans une revue hal-02317465 v1

Détection d’Isotopomères 2H-13C en Abondance Naturelle par RMN 2D Isotrope et Anisotrope, ou Comment Distinguer Expérimentalement une Molécule parmi 600 000?

Philippe Lesot , Olivier Lafon
Spectra Analyse, 2012, 287, pp.24-30
Article dans une revue hal-02317494 v1

Analytical contribution of NAD 2D-NMR spectroscopy in polypeptide mesophases to the investigation of triglycerides

Philippe Lesot , Zeinab Serhan , Christie Aroulanda , Isabelle Billault
Magnetic Resonance in Chemistry, 2012, 50, pp.S2-S11. ⟨10.1002/mrc.3855⟩
Article dans une revue istex hal-02311508 v1

Exploring the spectral enantiodiscrimination potential of a DNA-based orienting medium using deuterium NMR spectroscopy

Philippe Lesot , U. Venkateswara Reddy , N. Suryaprakash
Chemical Communications, 2011, 47 (42), pp.11736. ⟨10.1039/C1CC15097A⟩
Article dans une revue hal-02311046 v1

Conformation and Dynamics of 18-Membered Hexathiametacyclophanes: A Two Step Racemization as Studied by Deuterium NMR in Chiral Lyotropic Liquid Crystals

Philippe Lesot , Christie Aroulanda , Philippe Berdagué , Herbert Zimmermann , Zeev Luz
Journal of Physical Chemistry B, 2011, 115 (41), pp.11793-11804. ⟨10.1021/jp205958k⟩
Article dans une revue hal-02311044 v1

Fast and High-Resolution Stereochemical Analysis by Nonuniform Sampling and Covariance Processing of Anisotropic Natural Abundance 2D 2H NMR Datasets

Olivier Lafon , Bingwen Hu , Jean-Paul Amoureux , Philippe Lesot
Chemistry - A European Journal, 2011, 17 (24), pp.6716-6724. ⟨10.1002/chem.201100461⟩
Article dans une revue istex hal-02311041 v1

Enantiotopic discrimination in the deuterium NMR spectrum of solutes with S4 symmetry in chiral liquid crystals

Christie Aroulanda , Herbert Zimmermann , Zeev Luz , Philippe Lesot
The Journal of Chemical Physics, 2011, 134 (13), pp.134502. ⟨10.1063/1.3554640⟩
Article dans une revue hal-02311037 v1

Recent advances in the analysis of the site-specific isotopic fractionation of metabolites such as fatty acids using anisotropic natural-abundance H-2 NMR spectroscopy: application to conjugated linolenic methyl esters

Philippe Lesot , Zeinab Serhan , Isabelle Billault
Analytical and Bioanalytical Chemistry, 2011, 399 (3), pp.1187-1200. ⟨10.1007/s00216-010-4394-0⟩
Article dans une revue istex hal-02143481 v1

Recent advances in the analysis of the site-specific isotopic fractionation of metabolites such as fatty acids using anisotropic natural-abundance 2H NMR spectroscopy: application to conjugated linolenic methyl esters

Philippe Lesot , Zeinab Serhan , Isabelle Billault
Analytical and Bioanalytical Chemistry, 2011, 399 (3), pp.1187-1200. ⟨10.1007/s00216-010-4394-0⟩
Article dans une revue istex hal-02311033 v1

The conformation and orientational order of a 1,2-disubstituted ethane nematogenic molecule (I22) in liquid crystalline and isotropic phases studied by NMR spectroscopy

James Emsley , Philippe Lesot , Anne Lesage , Giuseppina de Luca , Denis Merlet et al.
Physical Chemistry Chemical Physics, 2010, 12 (12), pp.2895. ⟨10.1039/b915587b⟩
Article dans une revue istex hal-02310986 v1

Dynamic kinetic resolution of α-chloro β-keto esters and phosphonates: hemisynthesis of Taxotere® through Ru-DIFLUORPHOS asymmetric hydrogenation

Sébastien Prevost , Sebastien Gauthier , Maria Cristina Caño de Andrade , Céline Mordant , Ali Rhida Touati et al.
Tetrahedron: Asymmetry, 2010, 21 (11-12), pp.1436 - 1446. ⟨10.1016/j.tetasy.2010.05.017⟩
Article dans une revue istex hal-01664847 v1

Evolution of the Saupe order parameters of enantiomers from a racemic to a non-racemic liquid crystal solvent: an original light on the absolute configuration determination problem

J. Courtieu , C. Aroulanda , Philippe Lesot , A. Meddour , D. Merlet
Liquid Crystals, 2010, 37 (6-7), pp.903-912. ⟨10.1080/02678291003784164⟩
Article dans une revue hal-02311001 v1

Cationic Planar Chiral (η 6 -Arene)Mn(CO) 3 + Complexes: Resolution, NMR Study in Chiral-Oriented Solvents, and Applications to the Enantioselective Synthesis of 4-Substituted Cyclohexenones and (η6 -Phosphinoarene)Mn(CO)3+ Complexes

Antoine Eloi , Françoise Rose-Munch , Eric Rose , Ariane Pille , Philippe Lesot et al.
Organometallics, 2010, 29 (17), pp.3876-3886. ⟨10.1021/om100564v⟩
Article dans une revue hal-02316048 v1

Complete determination of natural site-specific enantio-isotopomeric excesses in linoleic acid using natural abundance deuterium 2D NMR in polypeptide mesophases

Zeinab Serhan , Laura Martel , Isabelle Billault , Philippe Lesot
Chemical Communications, 2010, 46 (35), pp.6599-6601. ⟨10.1039/c0cc01486a⟩
Article dans une revue istex hal-02143503 v1

Synthesis of 2-Trifluoromethyl-1,3-oxazolidines as Hydrolytically Stable Pseudoprolines

Grégory Chaume , Olivier Barbeau , Philippe Lesot , Thierry Brigaud
Journal of Organic Chemistry, 2010, 75 (12), pp.4135-4145. ⟨10.1021/jo100518t⟩
Article dans une revue hal-02310997 v1

Regio-defined amino[5]oxa- and thiahelicenes: A dramatic impact of the nature of the heteroatom on the helical shape and racemization barriers

Grégory Pieters , Anne Gaucher , Sylvain R A Marque , François Maurel , Philippe Lesot et al.
Journal of Organic Chemistry, 2010, 75 (6), pp.2096-2098. ⟨10.1021/jo1000127⟩
Article dans une revue hal-02310992 v1

Enantiodiscrimination of Flexible Cyclic Solutes Using NMR Spectroscopy in Polypeptide Chiral Mesophases: Investigation of cis -Decalin and THF

Christie Aroulanda , Olivier Lafon , Philippe Lesot
Journal of Physical Chemistry B, 2009, 113 (31), pp.10628-10640. ⟨10.1021/jp902233m⟩
Article dans une revue hal-02310982 v1

Natural abundance deuterium NMR spectroscopy: Developments and analytical applications in liquids, liquid crystals and solid phases

Philippe Lesot , Jacques Courtieu
Progress in Nuclear Magnetic Resonance Spectroscopy, 2009, 55 (2), pp.128-159. ⟨10.1016/j.pnmrs.2009.01.001⟩
Article dans une revue hal-02310981 v1

Analysis of enantiotopic discrimination in the NMR spectra of prochiral solutes in chiral liquid crystals by symmetry factorization of the Saupe ordering matrix

Philippe Lesot , Christie Aroulanda , Zeev Luz
The Journal of Chemical Physics, 2009, 131 (10), pp.104501. ⟨10.1063/1.3197853⟩
Article dans une revue hal-02310983 v1

Investigation of Fatty Acid Elongation and Desaturation Steps in Fusarium lateritium by Quantitative Two-dimensional Deuterium NMR Spectroscopy in Chiral Oriented Media

Vincent Baillif , Richard J. Robins , Steven Le Feunteun , Philippe Lesot , Isabelle Billault
Journal of Biological Chemistry, 2009, 284 (16), pp.10783-10792. ⟨10.1074/jbc.M807826200⟩
Article dans une revue hal-02143940 v1

Enantiodiscrimination in Deuterium NMR Spectra of Flexible Chiral Molecules with Average Axial Symmetry Dissolved in Chiral Liquid Crystals: The Case of Tridioxyethylenetriphenylene

Philippe Lesot , Olivier Lafon , Herbert Zimmermann , Zeev Luz
Journal of the American Chemical Society, 2008, 130 (27), pp.8754-8761. ⟨10.1021/ja800957a⟩
Article dans une revue istex hal-02310973 v1

Enantiomeric analysis using natural abundance deuterium 3D NMR spectroscopy in polypeptide chiral oriented media

Philippe Lesot , Olivier Lafon
Chemical Physics Letters, 2008, 458 (1-3), pp.219-222. ⟨10.1016/j.cplett.2008.04.065⟩
Article dans une revue istex hal-02310970 v1

RMN du deutérium en abondance naturelle dans les cristaux liquides chiraux : évolutions technologiques, avancées méthodologiques et nouvelles applications analytiques

Philippe Lesot
Spectra Analyse, 2008, 262, pp.16-22
Article dans une revue hal-02317421 v1

Combined analysis of C-18 unsaturated fatty acids using natural abundance deuterium 2D NMR spectroscopy in chiral oriented solvents

Philippe Lesot , Vincent Baillif , Isabelle Billault
Analytical Chemistry, 2008, 80 (8), pp.2963-2972. ⟨10.1021/ac702443b⟩
Article dans une revue istex hal-02143963 v1

Two aspects of the desymmetrization of selected prochiral aromatic or vinylic dihalides: enantioselective halogen–lithium exchange and prochiral recognition in chiral liquid crystals

Chun-An Fan , Benoit Ferber , Henri Kagan , Olivier Lafon , Philippe Lesot
Tetrahedron: Asymmetry, 2008, 19 (23), pp.2666-2677. ⟨10.1016/j.tetasy.2008.12.003⟩
Article dans une revue istex hal-02310976 v1

2H NMR Studies on Two-Homopolypeptide Lyotropic Enantiodiscriminating Mesophases: Experimental Quantification of Solute-Fiber Affinities

Philippe Lesot , Olivier Lafon , Christie Aroulanda , Ronald Y. Dong
Chemistry - A European Journal, 2008, 14 (13), pp.4082-4092. ⟨10.1002/chem.200701543⟩
Article dans une revue istex hal-00298353 v1

Structure, Formation, and Dynamics of Mo12 and Mo16 Oxothiomolybdenum Rings Containing Terephtalate Derivatives

Jean-François Lemonnier , Sébastien Floquet , Jérôme Marrot , Emmanuel Terazzi , Claude Piguet et al.
Chemistry - A European Journal, 2007, 13 (12), pp.3548-3557. ⟨10.1002/chem.200601369⟩
Article dans une revue istex hal-02310922 v1

Analysis of Intramolecular Dynamic Processes in Enantiomeric Diaryl Atropisomers and Related Derivatives by 2H NMR Spectroscopy in Polypeptide Liquid Crystals

Olivier Lafon , Philippe Lesot , Chun-An Fan , Henri b. Kagan
Chemistry - A European Journal, 2007, 13 (13), pp.3772-3786. ⟨10.1002/chem.200601284⟩
Article dans une revue istex hal-02310936 v1

Chiral Discrimination in the 13 C and 2 H NMR of the Crown and Saddle Isomers of Nonamethoxy-Cyclotriveratrylene in Chiral Liquid-Crystalline Solutions

Olivier Lafon , Philippe Lesot , Herbert Zimmermann , Raphy Poupko , Zeev Luz
Journal of Physical Chemistry B, 2007, 111 (32), pp.9453-9467. ⟨10.1021/jp070564q⟩
Article dans une revue istex hal-02310954 v1

Empirical determination of the absolute configuration of small chiral molecules using natural abundance 2H NMR in chiral liquid crystals

Latifa Ziani , Philippe Lesot , Abdelkhrim Meddour , Jacques Courtieu
Chemical Communications, 2007, 45, pp.4737. ⟨10.1039/b711493a⟩
Article dans une revue istex hal-02310959 v1

Homo- and heteronuclear 2D NMR approaches to analyse a mixture of deuterated unlike/like stereoisomers using weakly ordering chiral liquid crystals

Karim Ben Ali , Olivier Lafon , Herbert Zimmermann , Eric Guittet , Philippe Lesot
Journal of Magnetic Resonance, 2007, 187 (2), pp.205-215. ⟨10.1016/j.jmr.2007.04.007⟩
Article dans une revue istex hal-02310947 v1

Enantioselective synthesis of methyl-5(R)-fluorohept-6-ynoate

Vijaya Lingam Manthati , A. Sai Krishna Murthy , Frédéric Caijo , Delphine Drouin , Philippe Lesot et al.
Tetrahedron: Asymmetry, 2006, 17 (15), pp.2306-2310. ⟨10.1016/j.tetasy.2006.08.010⟩
Article dans une revue istex hal-02310918 v1

Study of molecular rotational isomerism using deuterium NMR in chiral oriented solvents

Philippe Lesot , Olivier Lafon , Henri Kagan , Chun-An Fan
Chemical Communications, 2006, 4, pp.389-391. ⟨10.1039/b514694a⟩
Article dans une revue istex hal-02310907 v1

Assignment of Absolute Configuration of Natural Abundance Deuterium Signals Associated with ( R )- and ( S )-Enantioisotopomers in a Fatty Acid Aligned in a Chiral Liquid Crystal: Enantioselective Synthesis and NMR Analysis

Vincent Baillif , Richard Robins , Isabelle Billault , Philippe Lesot
Journal of the American Chemical Society, 2006, 128 (34), pp.11180-11187. ⟨10.1021/ja0617892⟩
Article dans une revue istex hal-02310912 v1

Enantiomeric Analysis of Planar Chiral (η 6 -Arene)chromium Tricarbonyl Complexes using NMR in Oriented Solvents

Olivier Lafon , Philippe Lesot , Françoise Rose-Munch , Eric Rose
Organometallics, 2005, 24 (16), pp.4021-4028. ⟨10.1021/om050239u⟩
Article dans une revue istex hal-02310905 v1

Développement et Applications de la RMN du Deutérium en Abondance Naturelle dans les Cristaux Liquides Chiraux: Une autre Approche de l’Analyse en Chimie Organique

Philippe Lesot
Spectra Analyse, 2005, 242, pp.37-42
Article dans une revue hal-02317383 v1

Enantiomeric Analysis of Planar Chiral (η<sup>6</sup>-Arene)chromium Tricarbonyl Complexes using NMR in Oriented Solvents

Olivier Lafon , Philippe Lesot , Michaël Rivard , Murielle Chavarot-Kerlidou , Françoise Rose-Munch et al.
Organometallics, 2005, 24, pp.4021 - 4028. ⟨10.1021/om050239u⟩
Article dans une revue istex hal-04013449 v1

Deuterium 3D NMR experiments for analysing weakly aligned, isotopically enriched solutes

Olivier Lafon , Philippe Lesot
Chemical Physics Letters, 2005, 404 (1-3), pp.90-94. ⟨10.1016/j.cplett.2005.01.040⟩
Article dans une revue istex hal-02310889 v1

Theoretical and experimental investigation of 13C relayed 2H–2H-COSY 2D experiments: Application to the analysis of weakly aligned solutes

Olivier Lafon , Philippe Lesot
Journal of Magnetic Resonance, 2005, 174 (2), pp.254-264. ⟨10.1016/j.jmr.2005.02.011⟩
Article dans une revue istex hal-02310894 v1

Modified z-gradient filtering as a mean to obtain phased deuterium autocorrelation 2D NMR spectra in oriented solvents

Olivier Lafon , Denis Merlet , Jacques Courtieu , Philippe Lesot
Journal of Magnetic Resonance, 2004, 171 (1), pp.135-142. ⟨10.1016/j.jmr.2004.08.010⟩
Article dans une revue istex hal-02310847 v1

Heteronuclear selective refocusing 2D NMR experiments for the spectral analysis of enantiomers in chiral oriented solvents

Jonathan Farjon , Jean-Pierre Baltaze , Philippe Lesot , Denis Merlet , Jacques Courtieu
Magnetic Resonance in Chemistry, 2004, 42 (7), pp.594-599. ⟨10.1002/mrc.1399⟩
Article dans une revue hal-03008490 v1

Analysis of the13C NMR Spectra of Molecules, Chiral by Isotopic Substitution, Dissolved in a Chiral Oriented Environment: Towards the Absolute Assignment of the pro-R/pro-S Character of Enantiotopic Ligands in Prochiral Molecules

Philippe Lesot , Olivier Lafon , Jacques Courtieu , Philippe Berdagué
Chemistry - A European Journal, 2004, 10 (15), pp.3741-3746. ⟨10.1002/chem.200400065⟩
Article dans une revue istex hal-02310803 v1

Exploring the Analytical Potential of NMR Spectroscopy in Chiral Anisotropic Media for the Study of the Natural Abundance Deuterium Distribution in Organic Molecules

Philippe Lesot , Christie Aroulanda , Isabelle Billault
Analytical Chemistry, 2004, 76 (10), pp.2827-2835. ⟨10.1021/ac030385e⟩
Article dans une revue istex hal-03008466 v1

The effect of a chiral nematic solvent on the orientational order and conformational distribution of a flexible prochiral solute

James W. Emsley , Philippe Lesot , Jacques Courtieu , Denis Merlet
Physical Chemistry Chemical Physics, 2004, 6 (23), pp.5331. ⟨10.1039/b411203b⟩
Article dans une revue istex hal-02310857 v1

The orientational order and conformational distributions of the two enantiomers in a racemic mixture of a chiral, flexible molecule dissolved in a chiral nematic liquid crystalline solvent

James Emsley , Philippe Lesot , Denis Merlet
Physical Chemistry Chemical Physics, 2004, 6 (3), pp.522. ⟨10.1039/b312512b⟩
Article dans une revue istex hal-02310778 v1

New amino acid-based anionic surfactants and their use as enantiodiscriminating lyotropic liquid crystalline NMR solvents

Krystyna Baczko , Chantal Larpent , Philippe Lesot
Tetrahedron: Asymmetry, 2004, 15 (6), pp.971-982. ⟨10.1016/j.tetasy.2004.01.022⟩
Article dans une revue istex hal-02310787 v1

Efficient enantiodiscrimination of chiral monophosphine oxides and boranes by phosphorus coupled 13C NMR spectroscopy in the presence of chiral ordering agents

Michael Rivard , F. Guillen , Jean-Claude Fiaud , Christie Aroulanda , Philippe Lesot
Tetrahedron: Asymmetry, 2003, 14 (9), pp.1141-1152. ⟨10.1016/S0957-4166(03)00202-7⟩
Article dans une revue istex hal-02310631 v1

Efficient enantiodiscrimination of chiral monophosphine oxides and boranes by phosphorus coupled 13C NMR spectroscopy in the presence of chiral ordering agents

Michaël Rivard , F. Guillen , Jean-Claude Fiaud , Christie Aroulanda , Philippe Lesot
Tetrahedron: Asymmetry, 2003, 14 (9), pp.1141. ⟨10.1016/S0957-4166(03)00202-7⟩
Article dans une revue istex hal-01146992 v1

2D-NMR Strategy Dedicated to the Analysis of Weakly Ordered, Fully Deuterated Enantiomers in Chiral Liquid Crystals

Philippe Lesot , Muriel Sarfati , Denis Merlet , Bernard Ancian , James Emsley et al.
Journal of the American Chemical Society, 2003, 125 (25), pp.7689-7695. ⟨10.1021/ja021277x⟩
Article dans une revue istex hal-02310635 v1

Structural Ambiguities Revisited in Two Bridged Ring Systems Exhibiting Enantiotopic Elements, Using Natural Abundance Deuterium NMR in Chiral Liquid Crystals

Christie Aroulanda , Denis Merlet , Jacques Courtieu , Philippe Lesot
Journal of Physical Chemistry A, 2003, 107 (50), pp.10911-10918. ⟨10.1021/jp030137m⟩
Article dans une revue istex hal-02310640 v1

Investigation of SmI2-mediated cyclisation of δ-iodo-α,β-unsaturated esters by deuterium 2D NMR in oriented solvents

Hélène Villar , François Guibé , Christie Aroulanda , Philippe Lesot
Tetrahedron: Asymmetry, 2002, 13 (14), pp.1465-1475. ⟨10.1016/S0957-4166(02)00259-8⟩
Article dans une revue istex hal-02310609 v1

Enantiomeric and Enantiotopic Analysis of Cone-Shaped Compounds with C 3 and C 3 v Symmetry Using NMR Spectroscopy in Chiral Anisotropic Solvents

Philippe Lesot , Denis Merlet , Muriel Sarfati , Jacques Courtieu , Herbert Zimmermann et al.
Journal of the American Chemical Society, 2002, 124 (34), pp.10071-10082. ⟨10.1021/ja020269d⟩
Article dans une revue istex hal-02310599 v1

Enantiomeric excess measurements in weakly oriented chiral liquid crystal solvents through 2D 1H selective refocusing experiments

Jonathan Farjon , Denis Merlet , Philippe Lesot , Jacques Courtieu
Journal of Magnetic Resonance, 2002, 158 (1-2), pp.169-172. ⟨10.1016/S1090-7807(02)00070-8⟩
Article dans une revue istex hal-02310612 v1

Routine Use of Natural Abundance Deuterium NMR in a Polypeptidic Chiral Oriented Solvent for the Determination of the Enantiomeric Composition of Chiral Building Blocks

Arnaud Parenty , Jean-Marc Campagne , Christie Aroulanda , Philippe Lesot
Organic Letters, 2002, 4 (10), pp.1663-1666. ⟨10.1021/ol020038b⟩
Article dans une revue hal-00165644 v1

Résonance Magnétique Nucléaire du Deutérium en Abondance Naturelle dans les Cristaux Liquide Chiraux: Franchir une Nouvelle Frontière dans l'Analyse de la Chiralité

Philippe Lesot
Lettre du Département des Sciences Chimiques du CNRS, 2002, 78, pp.13-17
Article dans une revue hal-02321165 v1

First successful enantiomeric discrimination of chiral alkanes using NMR spectroscopy

Muriel Sarfati , Jacques Courtieu , Philippe Lesot
Chemical Communications, 2001, 13, pp.1113-1114. ⟨10.1039/b002806l⟩
Article dans une revue hal-02309085 v1

Enantiomeric recognition of chiral invertomers through NMR in chiral oriented phases: a study of cis-decalin

Muriel Sarfati , Christie Aroulanda , Jacques Courtieu , Philippe Lesot
Tetrahedron: Asymmetry, 2001, 12 (5), pp.737-744. ⟨10.1016/S0957-4166(01)00103-3⟩
Article dans une revue istex hal-02309129 v1

Determining Enantiomeric Purity by NMR: Deuterium 2D NMR at Natural Abundance in Weakly Oriented Chiral Liquid Crystals

Philippe Lesot , Muriel Sarfati , Denis Merlet , Jacques Courtieu , Bernard Ancian et al.
Bruker Report, 2001, 149, pp.29-33
Article dans une revue hal-02321012 v1

Enantiomeric recognition of chiral invertomers through NMR in chiral oriented phases: a study of cis-decalin

Muriel Sarfati , Christie Aroulanda , Jacques Courtieu , Philippe Lesot
Tetrahedron: Asymmetry, 2001, 12 (5), pp.737-744. ⟨10.1016/S0957-4166(01)00103-3⟩
Article dans une revue istex hal-02338088 v1

NMR Experimental Evidence of the Differentiation of Enantiotopic Directions in Cs and C2v Molecules Using Partially Oriented, Chiral Media

Christie Aroulanda , Denis Merlet , Jacques Courtieu , Philippe Lesot
Journal of the American Chemical Society, 2001, 123 (48), pp.12059-12066. ⟨10.1021/ja011685l⟩
Article dans une revue istex hal-02309135 v1

Highly enantioselective propargylic monofluorination established by carbon-13 and fluorine-19 NMR in chiral liquid crystals

Valérie Madiot , Philippe Lesot , Danielle Gree , Jacques Courtieu , René Grée
Chemical Communications, 2000, 2, pp.169-170. ⟨10.1039/A909012F⟩
Article dans une revue hal-02309109 v1

Theoretical and experimental aspects of enantiomeric differentiation using natural abundance multinuclear nmr spectroscopy in chiral polypeptide liquid crystals

Muriel Sarfati , Philippe Lesot , Denis Merlet , Jacques Courtieu
Chemical Communications, 2000, 21, pp.2069-2081. ⟨10.1039/B006244H⟩
Article dans une revue hal-02309126 v1

Deuterium NMR stereochemical analysis of threo–erythro isomers bearing remote stereogenic centres in racemic and non-racemic liquid crystalline solvents

Cécile Canlet , Denis Merlet , Philippe Lesot , Abdelkrim Meddour , Jacques Courtieu
Tetrahedron: Asymmetry, 2000, 11 (9), pp.1911-1918. ⟨10.1016/S0957-4166(00)00125-7⟩
Article dans une revue istex hal-02309123 v1

Description of natural abundance deuterium 2D-NMR experiments in weakly ordered liquid-crystalline solvents using a tailored cartesian spin-operator formalism

Denis Merlet , Muriel Sarfati , Bernard Ancian , Jacques Courtieu , Philippe Lesot
Physical Chemistry Chemical Physics, 2000, 2 (10), pp.2283-2290. ⟨10.1039/b000834f⟩
Article dans une revue hal-02309116 v1

Two-Dimensional Deuterium NMR Spectroscopy of Chiral Molecules Oriented in a Polypeptide Liquid Crystal: Applications for the Enantiomeric Analysis through Natural Abundance Deuterium NMR

Denis Merlet , Bernard Ancian , Jacques Courtieu , Philippe Lesot
Journal of the American Chemical Society, 1999, 121 (22), pp.5249-5258. ⟨10.1021/ja9837699⟩
Article dans une revue istex hal-02309106 v1

The relationship between molecular symmetry and second-rank orientational order parameters for molecules in chiral liquid crystalline solvents

Denis Merlet , James Emsley , Philippe Lesot , Jacques Courtieu
The Journal of Chemical Physics, 1999, 111 (15), pp.6890-6896. ⟨10.1063/1.479982⟩
Article dans une revue hal-02309108 v1

Double diastereoselection in asymmetric [2+3] cycloaddition of chiral oxazoline N-oxides: application to the kinetic resolution of a racemic α,β-unsaturated δ-lactone

Olivier Dirat , Cyrille Kouklovsky , Yves Langlois , Philippe Lesot , Jacques Courtieu
Tetrahedron: Asymmetry, 1999, 10 (16), pp.3197-3207. ⟨10.1016/S0957-4166(99)00317-1⟩
Article dans une revue istex hal-02309107 v1

Simplification of19F NMR Spectra of Liquid Crystalline Samples by Multiple-Pulse COSY Experiments

Philippe Lesot , James Emsley , Jean-Michel Ouvrard , Eirian Curzon
Journal of Magnetic Resonance, 1998, 133 (1), pp.166-172. ⟨10.1006/jmre.1998.1452⟩
Article dans une revue istex hal-02309101 v1

Analysis of natural abundance deuterium NMR spectra of enantiomers in chiral liquid crystals via 2D auto-correlation experiments

Denis Merlet , Bernard Ancian , William Smadja , Jacques Courtieu , Philippe Lesot
Chemical Communications, 1998, 21, pp.2301-2302. ⟨10.1039/A805020A⟩
Article dans une revue istex hal-02309103 v1

Structural–dynamical relationship in silica PEG hybrid gels

Philippe Lesot , Séverin Chapuis , Jean Pierre Bayle , Jacques Rault , Eric Lafontaine et al.
Journal of Materials Chemistry, 1998, 8 (1), pp.147-151. ⟨10.1039/A704983H⟩
Article dans une revue istex hal-02309086 v1

Quantitative Description of the Facial Discrimination of Molecules Containing a Prochiral Group by NMR in a Chiral Liquid Crystal

D. Merlet , A. Loewenstein , W. Smadja , J. Courtieu , Philippe Lesot
Journal of the American Chemical Society, 1998, 120 (5), pp.963-969. ⟨10.1021/ja9726466⟩
Article dans une revue istex hal-02309088 v1

Enantiomeric visualization using proton-decoupled natural abundance deuterium NMR in poly(γ-benzyl-l-glutamate) liquid crystalline solutions

Philippe Lesot , Denis Merlet , Aharon Loewenstein , Jacques Courtieu
Tetrahedron: Asymmetry, 1998, 9 (11), pp.1871-1881. ⟨10.1016/S0957-4166(98)00179-7⟩
Article dans une revue istex hal-02309102 v1

Steric Hindrance Influence of a Diazo Link upon Mesogenic Properties of some Ligands and Related Copper Complexes

Philippe Lesot , Felix Perez , Patrick Judeinstein , Jean Pierre Bayle , Hassan Allouchi et al.
Journal de Chimie Physique, 1997, 94, pp.1695-1714
Article dans une revue hal-02320964 v1

Proton-decoupled carbon-13 NMR spectroscopy in a lyotropic chiral nematic solvent as an analytical tool for the measurement of the enantiomeric excess

A. Meddour , P. Berdague , A. Hedli , J. Courtieu , Philippe Lesot
Journal of the American Chemical Society, 1997, 119 (19), pp.4502-4508. ⟨10.1021/ja964002o⟩
Article dans une revue istex hal-02324618 v1

Calculation of the Molecular Ordering Parameters of (±)-3-Butyn-2-ol Dissolved in an Organic Solution of Poly(γ-benzyl- l -glutamate)

Philippe Lesot , Denis Merlet , Jacques Courtieu , James Emsley , Tapio Rantala et al.
Journal of Physical Chemistry A, 1997, 101 (31), pp.5719-5724. ⟨10.1021/jp9709262⟩
Article dans une revue istex hal-02309087 v1

Discrimination and analysis of the NMR spectra of enantiomers dissolved in chiral liquid crystal solvents through 2D correlation experiments

Philippe Lesot , Denis Merlet , Jacques Courtieu , J. Emsley
Liquid Crystals, 1996, 21 (3), pp.427-435. ⟨10.1080/02678299608032851⟩
Article dans une revue hal-02308703 v1

Measurement and Analysis of the Molecular Ordering Tensors of Two Enantiomers Oriented in a Polypeptide Liquid Crystalline System

Philippe Lesot , Yves Gounelle , Denis Merlet , Aharon Loewenstein , Jacques Courtieu
The Journal of physical chemistry, 1995, 99 (40), pp.14871-14875. ⟨10.1021/j100040a042⟩
Article dans une revue istex hal-02309083 v1

Visualization of enantiomers in a polypeptide liquid-crystal solvent through carbon-13 NMR spectroscopy

Philippe Lesot , Denis Merlet , Abdelkrim Meddour , Jacques Courtieu , Aharon Loewenstein
Journal of the Chemical Society, Faraday Transactions, 1995, 91 (9), pp.1371. ⟨10.1039/ft9959101371⟩
Article dans une revue istex hal-02309082 v1

Coherent Reduction of Dipolar Interactions in Molecules Dissolved in Anisotropic Media Using a New Multiple-Pulse Sequence in a COSY Experiment

Philippe Lesot , J.M. Ouvrard , B.N. Ouvrard , J. Courtieu
Journal of magnetic resonance. Series A, 1994, 107 (2), pp.141-150. ⟨10.1006/jmra.1994.1061⟩
Article dans une revue istex hal-02309080 v1

Multiple-pulse COSY NMR spectroscopy of oriented molecules in thermotropic cholesteric

Philippe Lesot , F. Nielsen , J. Ouvrard , J. Courtieu
The Journal of physical chemistry, 1994, 98 (49), pp.12849-12855. ⟨10.1021/j100100a009⟩
Article dans une revue istex hal-02309081 v1

Prediction of Anisotropic NMR Parameters in a PBLG based Chiral Liquid Crystal A comparison between Experiments and Molecular Dynamics Simulations

Bernard Rousseau , Ambre Courteaud , Philippe Lesot
CHIRAFUN, GdR Chirafun, Sep 2024, Orsay, France
Communication dans un congrès hal-04928867 v1

Acquisition rapide de spectres RMN multidimensionnels de solides en utilisant des échantillonnages alternatifs

Olivier Lafon , Julien Trebosc , Eriks Kupče , Philippe Lesot , Jean-Paul Amoureux
Groupement d'Etudes de Résonance Magnétique (GERM), May 2019, Saint Pierre d’Oléron, France
Communication dans un congrès hal-04438434 v1

Contribution de la RMN 2D DAN anisotrope à la détermination du profil isotopique (D/H) i dans des biomarqueurs: étude de la miliacine

Philippe Berdagué , Jérémy Jacob , Valerie Terwilliger , Claude Lemilbeau , Philippe Lesot
Colloque RMN GBP-Ile de France, May 2015, Gif-sur-Yvette, France
Communication dans un congrès hal-01400951 v1

(D/H) Isotopic Fractionation by Anisotropic NAD 2D-NMR Spectroscopy: Exploiting the Analytical Wealth of Oriented Solvents to Investigate Molecules of Interest

Philippe Lesot , Philippe Berdagué , Jérémy Jacob
8th International Symposium on Isotopomers, Oct 2016, Nantes, France
Communication dans un congrès hal-01401863 v1

Conditions environnementales, biosynthèses, diagenèse : contribution analytique de la RMN 2H en milieu anisotrope

Philippe Berdagué , Jérémy Jacob , Valery J. Terwilliger , Claude Le Milbeau , Philippe Lesot
4èmes Journées Climat et Impacts, Nov 2016, Orsay, France
Communication dans un congrès hal-01689725 v1

Miliacin from broomcorn millet – a fossil molecule of multiple interests for archaeologists and paleoenvironmentalists

Jérémy Jacob , Anaëlle Simonneau , Nicolas Bossard , Claude Le Milbeau , Marlène Lavrieux et al.
Millet Cultivation in the Caucasus from the 6th to the 2nd mill BC: Origin and Development, Nov 2015, Lyon, France
Communication dans un congrès hal-01400923 v1
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Chiral imines on the wave: reactivity of <em>tert</em>-butyl acrylate and stereoselectivity determination using NMR in liquid crystals

Lucie Vandromme , Li Chen , Lai Wei , Franck Le Bideau , André Loupy et al.
MOL2NET, International Conference on Multidisciplinary Sciences, 2015, SCIForum, France. pp.1-18, ⟨10.3390/MOL2NET-1-a003⟩
Communication dans un congrès hal-02314359 v1
Image document

Hydrogen Isotope Profile of Methyl Groups in Miliacin (olean-18-en-3βol ME) by Natural Abundance Deuterium 2D-NMR Spectroscopy in liquid crystals

Philippe Berdagué , Philippe Lesot , Jérémy Jacob , Valery T. Terwilliger , Claude Le Milbeau
the 26th International Meeting on Organic Geochemistry (IMOG 2013), Sep 2013, Tenerife, Spain. 3p
Communication dans un congrès insu-00843521 v1

Methodological Study of the Peptide Coupling of the N-desactivated Stable Proline Surrogate CF3-pseudoproline

Grégory Chaume , Olivier Barbeau , Philippe Lesot , Emeric Miclet , Thierry Brigaud
32nd European Peptide Symposium, 2012, Sitges, France. pp.S58-S200, ⟨10.1002/psc.2449⟩
Communication dans un congrès hal-02316083 v1
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Specific Natural Isotope Fractionation Studied by 2H Nuclear Magnetic Resonance (SNIF-NMR): History, Developments, and Applications

Philippe Lesot , Gérald Remaud , Ben-Li Zhang
Handbook of Isotopologue Biogeochemistry, Springer Nature Singapore, pp.1-41, 2023, ⟨10.1007/978-981-10-7048-8_38-1⟩
Chapitre d'ouvrage hal-04215287 v1
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Combining Fast 2D NMR Methods and Oriented Media

Philippe Lesot , Olivier Lafon
Jean-Nicolas Dumez; Patrick Giraudeau. Fast 2D Solution-state NMR: Concepts and Applications, 1, The Royal Society of Chemistry, 2023, 978-1-83916-400-2. ⟨10.1039/BK9781839168062-00441⟩
Chapitre d'ouvrage hal-04207389 v1
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Anisotropic 1D/2D NMR in Molecular Analysis

Philippe Lesot , Roberto R. Gil
K. Ivanov; P.K. Madhu; G. Rajalakshmi. Two-Dimensional (2D) NMR Methods, Wiley, pp.209-296, 2023, ⟨10.1002/9781119806721.ch9⟩
Chapitre d'ouvrage hal-04218745 v1
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Nuclear Magnetic Resonance Spectroscopy-Applicable Elements—Hydrogen Isotopes: 2 H NMR

Philippe Lesot
Reference Module in Chemistry, Molecular Sciences and Chemical Engineering, 7, Elsevier, pp.152-167, 2018, ⟨10.1016/B978-0-12-409547-2.14084-3⟩
Chapitre d'ouvrage hal-02334009 v1

Isotope Ratio Monitoring by NMR. Part 1: Recent Advances

Gérald Remaud , Patrick Giraudeau , Philippe Lesot , Serge Akoka
Ed. G. Webb. Modern Magnetic Resonance, 2nd Edition, 1-25, Springer International Publishing, 2017, 978-3-319-28275-6. ⟨10.1007/978-3-319-28275-6⟩
Chapitre d'ouvrage hal-02308872 v1

Isotope Ratio Monitoring by NMR. Part 2: New Applications in the Field of Defining Biosynthesis

Richard J. Robins , Gérald Remaud , Isabelle Billault , Philippe Lesot
Ed. G. Webb. Modern Magnetic Resonance, 2nd Edition, Springer International Publishing, pp.1-26, 2017, 978-3-319-28275-6. ⟨10.1007/978-3-319-28275-6_9-1⟩
Chapitre d'ouvrage hal-02321193 v1

Natural Abundance Deuterium NMR Spectroscopy

Philippe Lesot , Olivier Lafon
Encyclopedia of Spectroscopy and Spectrometry, Elsevier, pp.1-14, 2016, ⟨10.1016/B978-0-12-409547-2.12110-9⟩
Chapitre d'ouvrage hal-02308860 v1

Rapport de Conjoncture du CoNRS 2014 (INC / Section 12)

Chantal Andraud , Philippe Belmont , J.M. Campagne , Gaëlle Chouraqui , Emmanuel Gras et al.
CNRS Editions, Paris,. Rapport de Conjoncture du CoNRS 2014, CNRS Editions, Paris,, pp.255-274, 2014, 978-2-271-08746-1
Chapitre d'ouvrage hal-02338362 v1

Deuterium NMR of Liquid-crystalline Samples at Natural Abundance

Philippe Lesot
Encyclopedia of Magnetic Resonance (eMagRes, 2 (3), John Wiley & Sons, Ltd, pp.315-334, 2013, 780470034590. ⟨10.1002/9780470034590⟩
Chapitre d'ouvrage hal-02316109 v1

Architectures moléculaires : synthèses, mécanismes et propriétés

Chantal Andraud , Janick Ardisson , Didier Bourissou , Elisabet Dunach , J.C. Guillemin et al.
Rapport de Conjoncture du Comité national de la recherche scientifique 2010, CNRS éditions, pp.231-242, 2011, 978-2-271-07263-4
Chapitre d'ouvrage hal-02338332 v1

Analytical Potentials of Natural Abundance Deuterium NMR Spectroscopy In Achiral Thermotropics and Polypeptide Chiral Liquid Crystals

Philippe Lesot , Christie Aroulanda
World Scientific Publishing Co. Pte. Ltd. NMR Spectroscopy of Liquid Crystals,, pp.37-78, 2010
Chapitre d'ouvrage hal-02317644 v1

Deuterium NMR of Liquid-crystalline Samples at Natural Abundance

Philippe Lesot
EMagRes (Encyclopedia of Magnetic Resonance), 9 (37), John Wiley & Sons, Ltd, pp.1943-1948, 2007, ⟨10.1002/9780470034590.emrstm1318⟩
Chapitre d'ouvrage hal-03008886 v1

Chiral Liquid Crystal NMR: a Tool for Enantiomeric Analysis

Jacques Courtieu , Philippe Lesot , Denis Merlet , Abdelkrim Meddour , Christie Aroulanda
Eds. D.M. Grant & R.K. Harris, J. Wiley & Sons. Encyclopedia of NMR: Advances in NMR", 1st print edition, 9, pp.497-505, 2002
Chapitre d'ouvrage hal-02321152 v1